2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium

Base Information

• Chemical Name: 2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium
• CAS No.: 201029-10-9
• Molecular Formula: C10H5N10O8+
• Molecular Weight: 393.2089
• Mol file: 201029-10-9.mol

Synonyms:2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium

Chemical Property of 2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium

There total 7 articles about 2,4,8,10-Tetranitro-7H-pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium inner salt (201029-05-2) → 2,4,8,10-tetranitropyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium inner salt (201029-10-9)

Guidance literature:

With sulfuric acid; nitric acid; at 80 ℃;

DOI:10.1016/S0040-4039(97)10311-2

Reference yield:

3-nitro-4(1H)-pyridinone (15590-90-6) → 2,4,8,10-tetranitropyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium inner salt (201029-10-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 91 percent / phosphorous pentachloride, phosphorous oxychloride / 3 h / Heating

2: 72 percent / Na₂CO₃ / dimethylsulfoxide / 5 h / 60 °C

3: 60 percent / triethyl phosphite / toluene / 20 h / Heating

4: 58 percent / HNO₃, H₂SO₄ / 80 °C

With phosphorus pentachloride; sulfuric acid; nitric acid; sodium carbonate; triethyl phosphite; trichlorophosphate; In dimethyl sulfoxide; toluene;

DOI:10.1016/S0040-4039(97)10311-2

Reference yield:

3,4-diaminopyridine (54-96-6) → 2,4,8,10-tetranitropyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium inner salt (201029-10-9)

Guidance literature:

Multi-step reaction with 4 steps

1: 86 percent / NaNO₂,CH₃CO₂H / 1 h / 10 - 25 °C

2: 51 percent / Na₂CO₃ / dimethylsulfoxide / 6 h / 80 °C

3: 74 percent / triethyl phosphite / toluene / 20 h / Heating

4: 58 percent / HNO₃, H₂SO₄ / 80 °C

With sulfuric acid; nitric acid; sodium carbonate; acetic acid; sodium nitrite; triethyl phosphite; In dimethyl sulfoxide; toluene;

DOI:10.1016/S0040-4039(97)10311-2

upstream raw materials:

pyrido[3'',4'':4',5'][1,2,3]triazolo[2',1':2,3][1,2,3]triazolo[4,5-b]pyridin-6-ium inner salt

3-nitro-4(1H)-pyridinone

3,4-diaminopyridine

1H-[1.2.3]triazolo-(4,5-c)pyridine