1-Methyl-1H-indole-3-carboxylic acid benzyl ester

Base Information

Chemical Name:1-Methyl-1H-indole-3-carboxylic acid benzyl ester
CAS No.:1033693-00-3
Molecular Formula:C17H15NO2
Molecular Weight:265.3065
Hs Code.:
Mol file:1033693-00-3.mol

Synonyms:Benzyl1-methyl-1H-indole-3-carboxylate;1-Methyl-1H-indole-3-carboxylic acid benzyl ester

Suppliers and Price of 1-Methyl-1H-indole-3-carboxylic acid benzyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1-METHYL-1H-INDOLE-3-CARBOXYLIC ACID BENZYL ESTER 95.00%
5MG
$ 498.63

Total 3 raw suppliers

Chemical Property of 1-Methyl-1H-indole-3-carboxylic acid benzyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

1-METHYL-1H-INDOLE-3-CARBOXYLIC ACID BENZYL ESTER 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-Methyl-1H-indole-3-carboxylic acid benzyl ester

There total 2 articles about 1-Methyl-1H-indole-3-carboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 603-76-9
1-methylindole

: 201230-82-2
carbon monoxide

: 100-51-6,185532-71-2
benzyl alcohol

: 1033693-00-3
benzyl 1-methyl-1H-indole-3-carboxylate

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; oxygen; copper diacetate; dimethyl sulfoxide; triphenylphosphine; In toluene; at 100 ℃; for 36h; under 760.051 Torr; regioselective reaction;
DOI:10.1002/chem.201101300

Reference yield:

: 120-72-9
indole

: 1033693-00-3
benzyl 1-methyl-1H-indole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide

1.2: 20 °C

2.1: bis-triphenylphosphine-palladium(II) chloride; oxygen; copper diacetate; dimethyl sulfoxide; triphenylphosphine / toluene / 36 h / 100 °C / 760.05 Torr

With bis-triphenylphosphine-palladium(II) chloride; oxygen; copper diacetate; dimethyl sulfoxide; triphenylphosphine; potassium hydroxide; In N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201101300