N-THIONYL-3-TRIFLUOROMETHYLANILINE

Base Information

• Chemical Name: N-THIONYL-3-TRIFLUOROMETHYLANILINE
• CAS No.: 68090-67-5
• Molecular Formula: C7H4F3NOS
• Molecular Weight: 207.176

Synonyms:N-sulfinyl-m-trifluoromethyl aniline;

Chemical Property of N-THIONYL-3-TRIFLUOROMETHYLANILINE

Chemical Property:

• PSA: 61.52000
• LogP: 3.59920

Purity/Quality:

99% ^*data from raw suppliers

1-(Sulfinylamino)-3-(trifluoromethyl)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-THIONYL-3-TRIFLUOROMETHYLANILINE

There total 1 articles about N-THIONYL-3-TRIFLUOROMETHYLANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

3-trifluoromethylaniline (98-16-8) → N-sulfinyl-3-(trifluoromethyl)aniline (68090-67-5)

Guidance literature:

With N-(chlorosulfinyl)imidazole; In dichloromethane; at -40 - 20 ℃; for 1.5h; Inert atmosphere;

DOI:10.1002/anie.200806110

Reference yield: 86.0%

4-bromo-DL-mandelic acid (6940-50-7) + N-sulfinyl-3-(trifluoromethyl)aniline (68090-67-5) → C15H11BrF3NO2 (1158519-41-5)

Guidance literature:

4-bromo-DL-mandelic acid; With 1,2,4-Triazole; In dichloromethane; at 20 ℃; for 0.5h; Inert atmosphere;

N-sulfinyl-3-(trifluoromethyl)aniline; In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1002/anie.200806110

Reference yield: 80.0%

(trifluoromethyl)trimethylsilane (81290-20-2) + N-sulfinyl-3-(trifluoromethyl)aniline (68090-67-5) → trifluoro-methanesulfinic acid (3-trifluoromethyl-phenyl)-amide

Guidance literature:

With tetramethylammonium fluoride; In 1,2-dimethoxyethane; at -60 - -50 ℃; for 2h;

DOI:10.1016/S0040-4039(02)00367-2

upstream raw materials:

3-trifluoromethylaniline

Downstream raw materials:

C₁₅H₁₁BrF₃NO₂

C₁₉H₁₄F₃NO₂

C₁₅H₁₀Cl₂F₃NO₂

C₁₉H₁₄F₃NO₂

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