Pyrrolo[2,1-b]oxazol-5(6H)-one, 7a-heptyltetrahydro-3-phenyl-, (3R-cis)- (9CI)

Base Information

Chemical Name:Pyrrolo[2,1-b]oxazol-5(6H)-one, 7a-heptyltetrahydro-3-phenyl-, (3R-cis)- (9CI)
CAS No.:132959-41-2
Molecular Formula:C19H27NO2
Molecular Weight:301.429
Hs Code.:

Synonyms:(+)-3-Phenyl-5-oxo-7a-heptyl-2,3,5,6,7,7a-hexahydropyrrolo[2,1-b]oxazole;

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Chemical Property of Pyrrolo[2,1-b]oxazol-5(6H)-one, 7a-heptyltetrahydro-3-phenyl-, (3R-cis)- (9CI)

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Technology Process of Pyrrolo[2,1-b]oxazol-5(6H)-one, 7a-heptyltetrahydro-3-phenyl-, (3R-cis)- (9CI)

There total 1 articles about Pyrrolo[2,1-b]oxazol-5(6H)-one, 7a-heptyltetrahydro-3-phenyl-, (3R-cis)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 22847-06-9
4-oxoundecanoic acid

: 56613-80-0
D-2-phenylglycinol

: 132959-41-2
(-)-(3R,7aS)-3-Phenyl-5-oxo-7a-heptyl-2,3,5,6,7,7a-hexahydropyrrolo<2,1-b>oxazole

Guidance literature:: In toluene; Heating;
DOI:10.1021/jo00007a011

Reference yield: 90.0%

: 132959-41-2
(-)-(3R,7aS)-3-Phenyl-5-oxo-7a-heptyl-2,3,5,6,7,7a-hexahydropyrrolo<2,1-b>oxazole

: 116830-36-5
(-)-N-<2-(1-Hydroxy-2(R)-phenylethyl)>-5(R)-heptyl-2-pyrrolidine

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In tetrahydrofuran; at -78 ℃;
DOI:10.1021/jo00007a011

Reference yield: 87.0%

: 132959-41-2
(-)-(3R,7aS)-3-Phenyl-5-oxo-7a-heptyl-2,3,5,6,7,7a-hexahydropyrrolo<2,1-b>oxazole

: 139564-36-6
(+)-N-<2-(1-Hydroxy-2(R)-phenylethyl)>-5(R)-heptyl-2-pyrrolidinone

Guidance literature:: With triethylsilane; titanium tetrachloride; In dichloromethane; Further byproducts given. Yields of byproduct given; a) -78 deg C, 1.5 h, b) r.t., 12 h;
DOI:10.1021/jo00032a012