10-Phosphonodecylphosphonic acid

Base Information

• Chemical Name: 10-Phosphonodecylphosphonic acid
• CAS No.: 5943-21-5
• Molecular Formula: C10H24O6P2
• Molecular Weight: 302.24
• European Community (EC) Number: 685-689-1
• DSSTox Substance ID: DTXSID20556271
• Nikkaji Number: J715.523I
• Wikidata: Q82437773
• Mol file: 5943-21-5.mol

Synonyms:1,10-Decyldiphosphonic acid;5943-21-5;10-PHOSPHONODECYLPHOSPHONIC ACID;1,10-Decanediphosphonic acid;1,10-Decanediylbisphosphonic acid;SCHEMBL630093;DTXSID20556271;MFCD18785729;1,10-Decyldiphosphonic acid, >97%;AKOS040768163;Decane-1,10-diylbis(phosphonic acid)

Chemical Property of 10-Phosphonodecylphosphonic acid

Chemical Property:

• Melting Point: 198-203°C
• PSA: 134.68000
• LogP: 2.46260
• XLogP3: 0.2
• Hydrogen Bond Donor Count: 4
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 11
• Exact Mass: 302.10481248
• Heavy Atom Count: 18
• Complexity: 265

Purity/Quality:

99% ^*data from raw suppliers

1,10-Decyldiphosphonic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C(CCCCCP(=O)(O)O)CCCCP(=O)(O)O
• Uses: 1,10-Decyldiphosphonic Acid is an anodic inhibitor used in corrosion protection by self assembly.

Technology Process of 10-Phosphonodecylphosphonic acid

There total 5 articles about 10-Phosphonodecylphosphonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

1,10-dibromodecane (4101-68-2) + triethyl phosphite (122-52-1) → 1,10-Diphosphono-decan (5943-21-5)

Guidance literature:

1,10-dibromodecane; triethyl phosphite; for 0.0833333h; Microwave irradiation;

With water; hydrogen bromide; Microwave irradiation;

DOI:10.1080/10426500903135543

Reference yield:

tetraethyl decane-1,10-diyldiphosphonate (5943-62-4) → 1,10-Diphosphono-decan (5943-21-5)

Guidance literature:

With hydrogenchloride;

DOI:10.1039/j39660000757

Reference yield:

1,10-dibromodecane (4101-68-2) → 1,10-Diphosphono-decan (5943-21-5)

Guidance literature:

Multi-step reaction with 2 steps

2: aq. HCl

With hydrogenchloride;

DOI:10.1039/j39660000757

upstream raw materials:

tetraethyl decane-1,10-diyldiphosphonate

1,10-dibromodecane

triethyl phosphite

Refernces

• 1、 Meziane, Dalila,Hardouin, Julie,Elias, Abdelhamid,Guenin, Erwann,Lecouvey, Marc. "Microwave michaelis-becker synthesis of diethyl phosphonates, tetraethyl diphosphonates, and their total or partial dealkylation". experimental part. p. 369 - 377. Retrieved 2010/07/16.