Di(2-ethylhexyl)dichlorosilane

Base Information

• Chemical Name: Di(2-ethylhexyl)dichlorosilane
• CAS No.: 1089687-03-5
• Molecular Formula: C16H34Cl2S
• Molecular Weight: 325.437
• Hs Code.: 29319090
• Mol file: 1089687-03-5.mol

Synonyms:Di(2-ethylhexyl)dichlorosilane; Dichlorodi(2-ethylhexyl)silane;

Chemical Property of Di(2-ethylhexyl)dichlorosilane

Chemical Property:

• Refractive Index: 1.4590 to 1.4630
• Boiling Point: 132-138°C / 1.5
• PSA: 0.00000
• Density: 0.924±0.06 g/cm3(Predicted)
• LogP: 7.33900
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

≥99% ^*data from raw suppliers

Dichlorobis(2-ethylhexyl)silane >95.0%(GC) ^*data from reagent suppliers

Safty Information:

• Statements: 10-23/24/35-36/37/38
• Safety Statements: 36/37/39-62-43-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Di(2-ethylhexyl)dichlorosilane

There total 3 articles about Di(2-ethylhexyl)dichlorosilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

trichloro(2-ethylhexyl)silane (222058-04-0) + 2-ethylhexylmagnesium bromide → dichloro-bis(2-ethylhexyl)silane (1089687-03-5)

Guidance literature:

In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja806687u

Reference yield: 71.0%

4,8-dihydrobenzo[1,2-b:4,5-b']dithiophene-4,8-dione (32281-36-0) → 3,6-dithiophen-2-yl-2,5-dihydropyrrolo[3,4-c]pyrrole-1,4-dione + dichloro-bis(2-ethylhexyl)silane (1089687-03-5)

Guidance literature:

In tetrahydrofuran;

Reference yield:

2-ethylhexylmagnesium bromide → dichloro-bis(2-ethylhexyl)silane (1089687-03-5)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium; tetrachlorosilane / water; tetrahydrofuran / 12 h / 20 °C

2: tetrahydrofuran / 6 h / -10 - 20 °C

With tetrachlorosilane; magnesium; In tetrahydrofuran; water;

upstream raw materials:

trichloro(2-ethylhexyl)silane

4,8-dihydrobenzo[1,2-b:4,5-b']dithiophene-4,8-dione

Downstream raw materials:

2,6-dibromo-4,4-bis(2-ethylhexyl)-4H-silolo[3,2-b:4,5-b']dithiophene

2,2′-bistrimethylstannyl-4,4′-bis-(2-ethylhexyl)dithieno[3,2-b:2′,3′-d]silole

4,4'-bis-(2-ethylhexyl)-dithieno[3,2-b:2',3'-d]silole

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