(E)-N-benzylidenebenzenesulfonamide

Base Information

Chemical Name:(E)-N-benzylidenebenzenesulfonamide
CAS No.:130552-90-8
Molecular Formula:C13H11NO2S
Molecular Weight:245.302
Hs Code.:
Mol file:130552-90-8.mol

Synonyms:N-Benzyl-2-butenamide;N-benzyl crotonamide;N-benzyl-but-2-enamide;N-benzylidene-benzenesulfonamide;N-benzenesulfonylbenzaldimine;

Suppliers and Price of (E)-N-benzylidenebenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of (E)-N-benzylidenebenzenesulfonamide

Chemical Property:

Melting Point:76-78℃
PSA：54.88000
LogP:3.57520

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (E)-N-benzylidenebenzenesulfonamide

There total 5 articles about (E)-N-benzylidenebenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 98-10-2
benzenesulfonamide

: 1125-88-8
benzaldehyde dimethyl acetal

: 130552-90-8
(E)-N-benzylidenebenzenesulfonamide

Guidance literature:: at 150 ℃;
DOI:10.1021/jo0485536

Reference yield:

: 14674-26-1
N-(α-p-Tosyl-benzyl)-benzolsulfonamid

: 130552-90-8
(E)-N-benzylidenebenzenesulfonamide

Guidance literature:: With water; sodium hydrogencarbonate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1055/s-2000-6232

Reference yield:

: 100-52-7
benzaldehyde

: 130552-90-8
(E)-N-benzylidenebenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: formic acid; H₂O / 12 h / 20 °C

2: NaHCO₃; H₂O / CH₂Cl₂ / 2 h / 20 °C

With water; sodium hydrogencarbonate; In formic acid; dichloromethane; water; 1: Condensation / 2: Elimination;
DOI:10.1055/s-2000-6232