BENZYL ALCOHOL-OD

Base Information

• Chemical Name: BENZYL ALCOHOL-OD
• CAS No.: 14915-25-4
• Molecular Formula: C6H5CH2OD
• Molecular Weight: 109.132
• Mol file: 14915-25-4.mol

Synonyms:

Chemical Property of BENZYL ALCOHOL-OD

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL ALCOHOL-OD

There total 12 articles about BENZYL ALCOHOL-OD which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

benzyl alcohol (100-51-6,185532-71-2) → benzyl alcohol-d (14915-25-4)

Guidance literature:

With d⁽⁴⁾-methanol; at 20 ℃; for 48h;

DOI:10.1039/d1cc01388b

Reference yield: 55.0%

benzaldehyde (100-52-7) → benzyl alcohol-d (14915-25-4)

Guidance literature:

With sodium borodeuteride; In deuteromethanol; Cooling with ice;

DOI:10.1021/jacs.5b09940

Reference yield:

deuterium sulfide (13536-94-2) + benzyl alcohol (100-51-6,185532-71-2) → benzyl alcohol-d (14915-25-4) + hydrogen sulfide (7783-06-4)

Guidance literature:

In further solvent(s); investigation of hydrogen ions change react. at -79°C in liqui D2S, mechanism discussed;;

upstream raw materials:

benzyl alcohol

allylbenzyloxy-t-butylmethylsilane

deuterium sulfide

benzaldehyde

Downstream raw materials:

benzyl alcohol

deuteriomethyl-benzene

toluene

benzaldehyde