Benzenecarbotelluroic acid, Te-[2-(hydroxyimino)-2-phenylethyl] ester

Base Information

• Chemical Name: Benzenecarbotelluroic acid, Te-[2-(hydroxyimino)-2-phenylethyl] ester
• CAS No.: 1236132-62-9
• Molecular Formula: C₁₅H₁₃NO₂Te
• Molecular Weight: 366.874
• Mol file: 1236132-62-9.mol

Synonyms:

Chemical Property of Benzenecarbotelluroic acid, Te-[2-(hydroxyimino)-2-phenylethyl] ester

Chemical Property:

Purity/Quality:

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Technology Process of Benzenecarbotelluroic acid, Te-[2-(hydroxyimino)-2-phenylethyl] ester

There total 1 articles about Benzenecarbotelluroic acid, Te-[2-(hydroxyimino)-2-phenylethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

potassium benzenecarbotelluroate (220867-00-5) + 2-bromo-1-phenyl-ethanone oxime (14181-72-7,17082-13-2,17082-14-3) → Te-acetophenone oxime benzenecarbotelluroate (1236132-62-9)

Guidance literature:

In tetrahydrofuran; acetonitrile; at -20 ℃; for 1h; Inert atmosphere;

DOI:10.1080/10426501003769728

Reference yield:

Te-acetophenone oxime benzenecarbotelluroate (1236132-62-9) → anti-O-benzoylacetophenone oxime (875537-86-3) + (E)-1-phenyl-ethanone o-benzoyloxime (18322-85-5)

Guidance literature:

With silica gel; In tetrahydrofuran; at 23 ℃; for 1h; Inert atmosphere;

DOI:10.1080/10426501003769728

upstream raw materials:

potassium benzenecarbotelluroate

2-bromo-1-phenyl-ethanone oxime

Downstream raw materials:

anti-O-benzoylacetophenone oxime

(E)-1-phenyl-ethanone o-benzoyloxime

Refernces