6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile

Base Information

Chemical Name:6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile
CAS No.:329348-61-0
Molecular Formula:C9H7ClN2O2
Molecular Weight:210.62
Hs Code.:2933399090
DSSTox Substance ID:DTXSID10368340
Wikidata:Q82154801
ChEMBL ID:CHEMBL1402879
Mol file:329348-61-0.mol

Synonyms:329348-61-0;6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile;6-chloro-5-formyl-1,4-dimethyl-2-oxo-1,2-dihydropyridine-3-carbonitrile;6-chloro-5-formyl-1,4-dimethyl-2-oxopyridine-3-carbonitrile;MLS001006158;CHEMBL1402879;SCHEMBL15331453;DTXSID10368340;HMS2706G10;STK819262;AKOS001051838;SMR000349267;CS-0279415;EN300-01070;SR-01000039248;SR-01000039248-1;Z56880546;F1673-6753

Suppliers and Price of 6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile 95+%
1g
$ 772.00

Chemenu
6-chloro-5-formyl-1,4-dimethyl-2-oxo-1,2-dihydropyridine-3-carbonitrile 95%
1g
$ 729.00

American Custom Chemicals Corporation
6-CHLORO-5-FORMYL-1,2-DIHYDRO-1,4-DIMETHYL-2-OXOPYRIDINE-3-CARBONITRILE 95.00%
1G
$ 1575.00

American Custom Chemicals Corporation
6-CHLORO-5-FORMYL-1,2-DIHYDRO-1,4-DIMETHYL-2-OXOPYRIDINE-3-CARBONITRILE 95.00%
5MG
$ 501.89

Alichem
6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile
1g
$ 621.72

Total 6 raw suppliers

Chemical Property of 6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile

Chemical Property:

PSA：62.86000
LogP:1.03128
Storage Temp.:2-8°C
XLogP3:0.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:210.0196052
Heavy Atom Count:14
Complexity:425

Purity/Quality:

95+% ^*data from raw suppliers

6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C(=O)N(C(=C1C=O)Cl)C)C#N

Technology Process of 6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile

There total 1 articles about 6-Chloro-5-formyl-1,2-dihydro-1,4-dimethyl-2-oxopyridine-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 27074-03-9
1,4-dimethyl-2,6-dioxo-1,2,3,6-tetrahydro-pyridine-3-carbonitrile

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 329348-61-0
6-Chloro-3-cyano-5-formyl-1,4-dimethylpyridin-2(1H)-one

Guidance literature:: With trichlorophosphate; at 65 - 70 ℃; for 7h;
DOI:10.1055/s-2001-9749

Reference yield:

: 329348-61-0
6-Chloro-3-cyano-5-formyl-1,4-dimethylpyridin-2(1H)-one

: 329348-63-2
3-Cyano-5-formyl-1,4-dimethyl-6-[(triphenylphosphoranylidene)amino]pyridin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaN₃ / methanol / 2 h / 25 °C

2: 89 percent / toluene / 0.5 h / 25 °C

With sodium azide; In methanol; toluene;
DOI:10.1055/s-2001-9749