5-Morpholinopicolinic acid

Base Information

Chemical Name:5-Morpholinopicolinic acid
CAS No.:1072103-29-7
Molecular Formula:C10H12N2O3
Molecular Weight:208.21
Hs Code.:2934999090
Mol file:1072103-29-7.mol

Synonyms:5-Morpholinopicolinic acid

Suppliers and Price of 5-Morpholinopicolinic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

ChemScene
5-Morpholinopicolinicacid 99.62%
1g
$ 444.00

ChemScene
5-Morpholinopicolinicacid 99.62%
250mg
$ 177.00

ChemScene
5-Morpholinopicolinicacid 99.62%
100mg
$ 97.00

ChemScene
5-Morpholinopicolinicacid 99.62%
5g
$ 2001.00

ChemScene
5-Morpholinopicolinicacid 99.62%
50mg
$ 75.00

Chemenu
5-Morpholinopicolinicacid 95%
1g
$ 580.00

American Custom Chemicals Corporation
5-MORPHOLINOPICOLINIC ACID 95.00%
5MG
$ 496.43

Ambeed
5-Morpholinopicolinicacid 95%
250mg
$ 182.00

Ambeed
5-Morpholinopicolinicacid 95%
100mg
$ 182.00

Ambeed
5-Morpholinopicolinicacid 95%
50mg
$ 97.00

Total 10 raw suppliers

Chemical Property of 5-Morpholinopicolinic acid

Chemical Property:

Boiling Point:446.1±45.0 °C(Predicted)
PKA:0.86±0.50(Predicted)
PSA：62.66000
Density:1.313±0.06 g/cm3(Predicted)
LogP:0.68140
Storage Temp.:2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-Morpholinopicolinicacid 99.62% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-Morpholinopicolinic acid

There total 8 articles about 5-Morpholinopicolinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1301214-68-5
4-[6-(piperidin-1-ylcarbonyl)pyridin-3-yl]morpholine

: 1072103-29-7
5-morpholinopicolinic acid

Guidance literature:: 4-[6-(piperidin-1-ylcarbonyl)pyridin-3-yl]morpholine; With potassium hydroxide; Reflux;

With hydrogenchloride; In water;

Reference yield:

: 60891-70-5
1,3-diethyl 2-(5-nitropyridin-2-yl)propanedioate

: 1072103-29-7
5-morpholinopicolinic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: nitric acid / 15 h / Reflux

2.1: sulfuric acid / 5 h / Reflux

3.1: 1 h / Reflux

4.1: hydrogen / palladium 10% on activated carbon / acetic acid / 760.05 Torr

5.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

5.2: 0.25 h

6.1: sodium t-butanolate / palladium diacetate; johnphos / toluene / 2 h / 95 °C / Inert atmosphere

7.1: potassium hydroxide / Reflux

With hydrogenchloride; sulfuric acid; hydrogen; nitric acid; potassium hydroxide; sodium t-butanolate; sodium nitrite; palladium 10% on activated carbon; palladium diacetate; johnphos; In water; acetic acid; toluene;

Reference yield:

: 4548-45-2
2-chloro-5-nitropyridine

: 1072103-29-7
5-morpholinopicolinic acid

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil

1.2: 2 h / Reflux

2.1: nitric acid / 15 h / Reflux

3.1: sulfuric acid / 5 h / Reflux

4.1: 1 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / acetic acid / 760.05 Torr

6.1: hydrogenchloride; sodium nitrite / water / 0.17 h / 0 °C

6.2: 0.25 h

7.1: sodium t-butanolate / palladium diacetate; johnphos / toluene / 2 h / 95 °C / Inert atmosphere

8.1: potassium hydroxide / Reflux

With hydrogenchloride; sulfuric acid; hydrogen; nitric acid; sodium hydride; potassium hydroxide; sodium t-butanolate; sodium nitrite; palladium 10% on activated carbon; palladium diacetate; johnphos; In tetrahydrofuran; water; acetic acid; toluene; mineral oil;