methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

Base Information

Chemical Name:methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate
CAS No.:1193244-87-9
Molecular Formula:C6H7IN2O2
Molecular Weight:266.03645
Hs Code.:
Mol file:1193244-87-9.mol

Synonyms:methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate;5-Iodo-1-methyl-1H-pyrazole-3-carboxylic acid methyl ester

Suppliers and Price of methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Methyl5-iodo-1-methyl-1H-pyrazole-3-carboxylate 95+%
1g
$ 635.00

Chemenu
Methyl5-iodo-1-methyl-1H-pyrazole-3-carboxylate 95%
1g
$ 594.00

American Custom Chemicals Corporation
METHYL 5-IODO-1-METHYL-1H-PYRAZOLE-3-CARBOXYLATE 95.00%
5MG
$ 505.00

Alichem
Methyl5-iodo-1-methyl-1H-pyrazole-3-carboxylate
1g
$ 522.24

Total 11 raw suppliers

Chemical Property of methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

Chemical Property:

PSA：44.12000
LogP:0.81130
Storage Temp.:2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

Methyl5-iodo-1-methyl-1H-pyrazole-3-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

There total 2 articles about methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 92406-53-6
methyl 5-amino-1-methyl-1H-pyrazole-3-carboxylate

: 1193244-87-9
methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

Guidance literature:: With acetic acid; potassium iodide; sodium nitrite; In water; at 0 ℃; for 3h;

Reference yield:

: 1227409-70-2
methyl 3-cyano-2-sodiumoxy-2-propenoate

: 1193244-87-9
methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 48 h / 18 - 25 °C

2: potassium iodide; sodium sulfite; acetic acid / water / 3 h / 0 °C

With acetic acid; potassium iodide; sodium sulfite; In methanol; water;

Reference yield:

: 1193244-87-9
methyl 5-iodo-1-methyl-1H-pyrazole-3-carboxylate

: 1227409-77-9
1-methyl-5-(quinolin-3-yl)-1H-pyrazol-3-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: tricyclohexylphosphine; potassium phosphate / tris-(dibenzylideneacetone)dipalladium⁽⁰⁾ / 1,4-dioxane / 15 h / 100 °C

2.1: sodium hydroxide / methanol / 2 h / 75 °C

2.2: 18 - 25 °C / pH 6 - 7

With potassium phosphate; sodium hydroxide; tricyclohexylphosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In 1,4-dioxane; methanol;