3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE

Base Information

• Chemical Name: 3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE
• CAS No.: 941271-13-2
• Molecular Formula: C16H17IN2O2
• Molecular Weight: 396.228
• Mol file: 941271-13-2.mol

Synonyms:3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE;tert-butyl 4-iodo-6-phenylpyridin-3-ylcarbamate

Chemical Property of 3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE

Chemical Property:

• Boiling Point: 418.6±45.0 °C(Predicted)
• PKA: 11.92±0.70(Predicted)
• PSA: 51.22000
• Density: 1.529±0.06 g/cm3(Predicted)
• LogP: 4.77320
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

tert-Butyl 4-iodo-6-phenylpyridin-3-ylcarbamate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE

There total 1 articles about 3-N-BOC-AMINO-4-IODO-6-PHENYLPYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

(6-phenylpyridin-3-yl)carbamic acid ter-butyl ester (849353-27-1) → (4-iodo-6-phenylpyridin-3-yl)carbamic acid ter-butyl ester (941271-13-2)

Guidance literature:

(6-phenylpyridin-3-yl)carbamic acid ter-butyl ester; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; at -78 ℃; for 0.25h;

at -10 ℃; for 3h;

With iodine; In tetrahydrofuran; diethyl ether; at -78 ℃; for 2h;

Reference yield:

6-(5-fluoro-2-methylphenyl)-6-methyl-4-trifluoromethylhept-1-yn-4-ol (849354-28-5) + (4-iodo-6-phenylpyridin-3-yl)carbamic acid ter-butyl ester (941271-13-2) → C32H34F4N2O3

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h;

DOI:10.1021/ml500387y

upstream raw materials:

(6-phenylpyridin-3-yl)carbamic acid ter-butyl ester

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