4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenylacetic acid

Base Information

• Chemical Name: 4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenylacetic acid
• CAS No.: 77357-10-9
• Molecular Formula: C₁₄H₁₂N₂O₅S
• Molecular Weight: 320.326
• Hs Code.: 2933399090
• Mol file: 77357-10-9.mol

Synonyms:4-(3’-nitro-2’-pyridinesulfenyloxymethyl)phenylacetic acid

Chemical Property of 4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenylacetic acid

Chemical Property:

• Vapor Pressure: 3.7E-12mmHg at 25°C
• Boiling Point: 532.2°C at 760 mmHg
• Flash Point: 275.7°C
• PSA: 130.54000
• Density: 1.46g/cm³
• LogP: 3.36400

Purity/Quality:

99%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenylacetic acid

There total 1 articles about 4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenylacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3-nitro-2-pyridinesulfenyl chloride (68206-45-1) + 4-hydroxymethylphenylacetic acid (73401-74-8) → 3,3’-dinitro-2,2’-dipyridinyl disulfide (4282-19-3) + 4-(3'-nitro-2'-pyridinesulfenyloxymethyl)phenyl acetic acid (77357-10-9)

Guidance literature:

With triethylamine; In dichloromethane; ethyl acetate; for 1h; Ambient temperature;

upstream raw materials:

3-nitro-2-pyridinesulfenyl chloride

4-hydroxymethylphenylacetic acid

Refernces