Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate

Base Information

Chemical Name:Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate
CAS No.:344361-90-6
Molecular Formula:C₉H₁₂N₂O₃S
Molecular Weight:228.272
Hs Code.:2933599090
Mol file:344361-90-6.mol

Synonyms:Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate

Suppliers and Price of Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
Ethyl4-Methyl-2-(methylthio)-6-oxo-1,6-dihydropyrimidine-5-carboxylate 95+%
1g
$ 281.00

Chemenu
Ethyl4-Methyl-2-(methylthio)-6-oxo-1,6-dihydropyrimidine-5-carboxylate 95%
5g
$ 439.00

American Custom Chemicals Corporation
ETHYL-4-METHYL-2-(METHYLTHIO)-6-OXO-1,6-DIHYDROPYRIMIDINE-5-CARBOXYLATE 95.00%
5MG
$ 505.11

AK Scientific
Ethyl4-methyl-2-(methylthio)-6-oxo-1,6-dihydropyrimidine-5-carboxylate
5g
$ 728.00

Total 20 raw suppliers

Chemical Property of Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate

Chemical Property:

Boiling Point:342.1±52.0 °C(Predicted)
PKA:6.92±0.50(Predicted)
PSA：97.61000
Density:1.33±0.1 g/cm3(Predicted)
LogP:1.38920
Storage Temp.:2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

Ethyl4-Methyl-2-(methylthio)-6-oxo-1,6-dihydropyrimidine-5-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate

There total 7 articles about Ethyl 4-Methyl-2-(Methylthio)-6-oxo-1,6-dihydropyriMidine-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.6%

: 583878-41-5
ethyl 4-methyl-2-(methylsulfanyl)-6-oxo-1,4,5,6-tetrahydro-5-pyrimidinecarboxylate

: 344361-90-6
5-ethoxycarbonyl-6-methyl-2-methylsulfanylpyrimidin-4(3H)-one

Guidance literature:: With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In 1,4-dioxane; at 90 ℃; for 3h;

Reference yield: 84.0%

: 36239-09-5
ethyl chlorocarbonylacetate

: {[(E)-[1-(dimethylamino)ethylidene]amino](methylsulfanyl)methylidene}azanium iodide

: 344361-90-6
5-ethoxycarbonyl-6-methyl-2-methylsulfanylpyrimidin-4(3H)-one

Guidance literature:: ethyl chlorocarbonylacetate; {[(E)-[1-(dimethylamino)ethylidene]amino](methylsulfanyl)methylidene}azanium iodide; In dichloromethane; at 20 ℃; for 4h;

With triethylamine;
DOI:10.1002/jhet.5570380113

Reference yield: 78.0%

: 583878-41-5
ethyl 4-methyl-2-(methylsulfanyl)-6-oxo-1,4,5,6-tetrahydro-5-pyrimidinecarboxylate

: 344361-90-6
4-hydroxy-6-methyl-2-methylsulfanyl-pyrimidine-5-carboxylic acid ethyl ester

Guidance literature:: ethyl 4-methyl-2-(methylsulfanyl)-6-oxo-1,4,5,6-tetrahydro-5-pyrimidinecarboxylate; With N-Bromosuccinimide; potassium carbonate; dibenzoyl peroxide; In tetrachloromethane; for 0.75h; Reflux;

With hydrogenchloride; In tetrachloromethane; water; at 20 ℃;