5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro-

Base Information

Chemical Name:5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro-
CAS No.:40443-01-4
Molecular Formula:C17H15Cl
Molecular Weight:254.75
Hs Code.:
Mol file:40443-01-4.mol

Synonyms:5-(2-Chloro-ethylidene)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene;5-<β-Chlor-aethyliden>-5H-dibenzo-10,11-dihydro-cyclohepten;10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-Δ5,β-ethylchlorid;5-(2-chloroethylidene)-10,11-dihydro-5H-dibenzo[a,d]cycloheptene;10,11-Dihydro-5H-dibenzocyclohepten-Δ5,β-ethylchlorid;

Suppliers and Price of 5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-(2-Chloroethylidene)-10,11-dihydro-5H-Dibenzo[a,d]cycloheptene
10mg
$ 1020.00

TRC
5-(2-Chloroethylidene)-10,11-dihydro-5H-Dibenzo[a,d]cycloheptene
5mg
$ 525.00

TRC
5-(2-Chloroethylidene)-10,11-dihydro-5H-Dibenzo[a,d]cycloheptene
1mg
$ 120.00

Total 1 raw suppliers

Chemical Property of 5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro-

Chemical Property:

Melting Point:93 - 96 °C
PSA：0.00000
LogP:4.45570

Purity/Quality:

98% ^*data from raw suppliers

5-(2-Chloroethylidene)-10,11-dihydro-5H-Dibenzo[a,d]cycloheptene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Uses 5-(2-Chloroethylidene)-10,11-dihydro-5H-Dibenzo[a,d]cycloheptene is used as a regeant in the synthesis of [(dihydrodibenzocyclohepthylidene)ethyl]piperazine derivatives which exhibit vasodilatory activity similar to common drugs such as cinnarizine and flunarizine. It may also be used in the preparation of N-(dihydrodibenzocycloheptenylideneethyl)ephedrines which are anti-ulcer agents.

Technology Process of 5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro-

There total 3 articles about 5H-Dibenzo[a,d]cycloheptene, 5-(2-chloroethylidene)-10,11-dihydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2732-90-3
5-methylene-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

: 40443-01-4
2-chloro-1-(10,11-dihydrodibenzo-(a,d)-cyclohept-5-yliden)-ethane

Guidance literature:: With acetic acid; paraformaldehyde;

Reference yield:

: 3241-96-1
10,11-Dihydro-5-ethenyl-5H-dibenzocyclohepten-5-ol

: 40443-01-4
2-chloro-1-(10,11-dihydrodibenzo-(a,d)-cyclohept-5-yliden)-ethane

Guidance literature:: With hydrogenchloride; In acetic acid;
DOI:10.1021/jm00333a051

Reference yield:

: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

: 40443-01-4
2-chloro-1-(10,11-dihydrodibenzo-(a,d)-cyclohept-5-yliden)-ethane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran

2: HCl / CHCl₃

With hydrogenchloride; In tetrahydrofuran; chloroform;
DOI:10.1002/jlcr.2590080312