5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene-

Base Information Edit

Chemical Name:5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene-
CAS No.:2732-90-3
Molecular Formula:C16H14
Molecular Weight:206.287
Hs Code.:
Mol file:2732-90-3.mol

Synonyms:5-methenedibenzo[a,e]suberane;5-methylene-5H-dibenzo[a,d]cycloheptane;5-Methylen-10,11-dihydro-5H-dibenzo[a,d]cyclohepten;5-methylene10,11-dihydro-5H-dibenzo[a,d]cycloheptene;10,11-dihydro-5-methylene-5H-dibenzo[a,d]cycloheptene;

Suppliers and Price of 5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene-

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
5-Methylene-10,11-dihydro-5H-dibenzo[a,d][7]annulene ≥95%
5g
$ 750.00

Total 1 raw suppliers

Chemical Property of 5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene- Edit

Chemical Property:

Melting Point:67-68 °C(Solv: methanol (67-56-1))
Boiling Point:324.5±27.0 °C(Predicted)
PSA：0.00000
Density:1.07±0.1 g/cm3(Predicted)
LogP:3.84670

Purity/Quality:

98% ^*data from raw suppliers

5-Methylene-10,11-dihydro-5H-dibenzo[a,d][7]annulene ≥95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene-

There total 19 articles about 5H-Dibenzo[a,d]cycloheptene, 10,11-dihydro-5-methylene- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

: 1779-49-3
Methyltriphenylphosphonium bromide

: 2732-90-3
5-methylene-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

Guidance literature:: With potassium-t-butoxide; In diethyl ether; at 20 ℃; for 1h;
DOI:10.1021/jo990626b

Reference yield: 84.0%

: 1210-35-1
10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one

: methyl magnesium ⁽¹⁺⁾; bromide

: 2732-90-3
5-methylene-10,11-dihydro-5H-dibenzo[a,d]cycloheptene

Guidance literature:: 10,11-Dihydro-5H-dibenzo[a,d]cyclohepten-5-one; methyl magnesium ⁽¹⁺⁾; bromide; In tetrahydrofuran; diethyl ether; at 0 - 20 ℃; for 2h;

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃;