Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl-

Base Information

Chemical Name:Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl-
CAS No.:1257248-17-1
Molecular Formula:C33H25N
Molecular Weight:435.568
Hs Code.:

Synonyms:

Suppliers and Price of Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 2 raw suppliers

Chemical Property of Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl-

There total 2 articles about Indeno[2,1-b]carbazole, 5-[1,1'-biphenyl]-4-yl-5,7-dihydro-7,7-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.1%

: 92-66-0
4-bromo-1,1'-biphenyl

: 1257220-47-5
12,12-dimethyl-10,12-dihydro-10-azaindeno[2,1-b]fluorene

: 1257248-17-1
10-(biphenyl-4-yl)-12,12-dimethyl-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: With 3,5-ditertbutyl salicylic acid; copper; potassium carbonate; sodium hydrogensulfite; at 190 ℃; for 26h; Inert atmosphere;

Reference yield:

: 1357150-72-1
N-(2-bromophenyl)-9,9-dimethyl-9H-fluoren-2-amine

: 1257248-17-1
10-(biphenyl-4-yl)-12,12-dimethyl-10,12-dihydroindeno[2,1-b]carbazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium acetate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / N,N-dimethyl-formamide / 11 h / 100 °C / Inert atmosphere

2: sodium hydrogensulfite; copper; 3,5-ditertbutyl salicylic acid; potassium carbonate / 26 h / 190 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 3,5-ditertbutyl salicylic acid; potassium acetate; copper; potassium carbonate; sodium hydrogensulfite; In N,N-dimethyl-formamide;