3-[4-(2,3-Dichlorophenyl)-1-piperazinyl]-1-propanol

Base Information

• Chemical Name: 3-[4-(2,3-Dichlorophenyl)-1-piperazinyl]-1-propanol
• CAS No.: 131732-09-7
• Molecular Formula: C₁₃H₁₈Cl₂N₂O
• Molecular Weight: 289.205

Synonyms:1-Piperazinepropanol, 4-(2,3-dichlorophenyl)-;3-[4-(2,3-Dichlorophényl)-1-pipérazinyl]-1-propanol;

Chemical Property of 3-[4-(2,3-Dichlorophenyl)-1-piperazinyl]-1-propanol

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-[4-(2,3-Dichlorophenyl)-1-piperazinyl]-1-propanol

There total 1 articles about 3-[4-(2,3-Dichlorophenyl)-1-piperazinyl]-1-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(2,3-dichlorophenyl)-piperazine hydrochloride (119532-26-2,864512-47-0) + 1-bromo-3-propanol (627-18-9) → 3-(4-(2,3-dichlorophenyl)piperazin-1-yl)propan-1-ol (131732-09-7)

Guidance literature:

With potassium carbonate; In acetonitrile; for 5h; Reflux;

DOI:10.1002/cmdc.201900439

Reference yield:

methanesulfonyl chloride (124-63-0) + 3-(4-(2,3-dichlorophenyl)piperazin-1-yl)propan-1-ol (131732-09-7) → 3-(4-(2,3-dichlorophenyl)piperazin-1-yl)propyl methanesulfonate

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Cooling with ice;

DOI:10.1002/cmdc.201900439

Reference yield:

3-(4-(2,3-dichlorophenyl)piperazin-1-yl)propan-1-ol (131732-09-7) + urethane (51-79-6) → 1-(3-carbamoyloxy-propyl)-4-(2,3-dichloro-phenyl)-piperazine (100793-07-5)

Guidance literature:

With aluminum isopropoxide; toluene;

upstream raw materials:

1-(2,3-dichlorophenyl)-piperazine hydrochloride

1-bromo-3-propanol

Downstream raw materials:

1-(3-carbamoyloxy-propyl)-4-(2,3-dichloro-phenyl)-piperazine

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