Technology Process of 4-(Benzyloxy)-2-[(3-methyl-2-buten-1-yl)oxy]benzaldehyde
There total 2 articles about 4-(Benzyloxy)-2-[(3-methyl-2-buten-1-yl)oxy]benzaldehyde which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; potassium iodide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
Large scale reaction;
DOI:10.3987/COM-10-11962
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate; potassium iodide / acetonitrile / 12 h / 60 °C / Large scale reaction
2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 3 h / 20 °C / Large scale reaction
With
sodium hydrogencarbonate; potassium carbonate; potassium iodide;
In
N,N-dimethyl-formamide; acetonitrile;
DOI:10.3987/COM-10-11962
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.5 h / -30 °C
1.2: 2 h / -30 °C
2.1: N,N-diethylaniline / 3 h / 215 °C / Inert atmosphere
3.1: aluminum (III) chloride; N,N-diethylaniline / dichloromethane / -10 - 0 °C
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0 - 20 °C
4.2: 16 h / 20 °C
With
aluminum (III) chloride; n-butyllithium; diisopropylamine; 3-chloro-benzenecarboperoxoic acid; N,N-diethylaniline;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.3987/COM-10-11962
