3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile

Base Information

Chemical Name:3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile
CAS No.:1153326-39-6
Molecular Formula:C15H15N3O
Molecular Weight:253.304
Hs Code.:
DSSTox Substance ID:DTXSID10656113
Nikkaji Number:J2.879.811C

Synonyms:1153326-39-6;SCHEMBL21382629;DTXSID10656113;3-Amino-4-(4-methoxybenzylamino)benzonitrile;3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile

Suppliers and Price of 3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile

Chemical Property:

XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:253.121512110
Heavy Atom Count:19
Complexity:317

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC=C(C=C1)CNC2=C(C=C(C=C2)C#N)N

Technology Process of 3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile

There total 1 articles about 3-Amino-4-{[(4-methoxyphenyl)methyl]amino}benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2393-23-9
4-methoxy-benzylamine

: 1153326-39-6
3-amino-4-((4-methoxybenzyl)amino)benzonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / N,N-dimethyl-formamide / 12 h / 20 °C

2: ammonium chloride; zinc / tetrahydrofuran / 3 h / 0 - 65 °C

With sodium hydrogencarbonate; ammonium chloride; zinc; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield: 59.0%

: 1153326-39-6
3-amino-4-((4-methoxybenzyl)amino)benzonitrile

: 1254833-73-2
C₁₅H₁₃N₃O₃S

Guidance literature:: With SULFAMIDE; In diethylene glycol dimethyl ether; at 160 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.07.173