Benzenamine, 3-chloro-4-(1H-indazol-4-yloxy)-

Base Information

• Chemical Name: Benzenamine, 3-chloro-4-(1H-indazol-4-yloxy)-
• CAS No.: 1033810-14-8
• Molecular Formula: C₁₃H₁₀ClN₃O
• Molecular Weight: 259.695
• Hs Code.: 2933990090
• Mol file: 1033810-14-8.mol

Synonyms:BenzenaMine, 3-chloro-4-(1H-indazol-4-yloxy)-;3-Chloro-4-(1H-indazol-4-yloxy)aniline;4-((1H-Indazol-4-yl)oxy)-3-chloroaniline

Chemical Property of Benzenamine, 3-chloro-4-(1H-indazol-4-yloxy)-

Chemical Property:

• PSA: 63.93000
• LogP: 4.17200
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-((1H-Indazol-4-yl)oxy)-3-chloroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenamine, 3-chloro-4-(1H-indazol-4-yloxy)-

There total 4 articles about Benzenamine, 3-chloro-4-(1H-indazol-4-yloxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C13H8ClN3O3 → 3-chloro-4-(1H-indazol-4-yloxy)aniline (1033810-14-8)

Guidance literature:

With platinum on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 4h;

DOI:10.1021/jm300185p

Reference yield:

4-hydroxyindazole (81382-45-8) → 3-chloro-4-(1H-indazol-4-yloxy)aniline (1033810-14-8)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

2: platinum on carbon; hydrogen / ethyl acetate / 4 h / 20 °C

With platinum on carbon; hydrogen; potassium carbonate; In ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1021/jm300185p

Reference yield:

4-aminoindazole (41748-71-4) → 3-chloro-4-(1H-indazol-4-yloxy)aniline (1033810-14-8)

Guidance literature:

Multi-step reaction with 3 steps

1: sulfuric acid; sodium nitrite / water / 15 h / 0 - 100 °C

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C

3: platinum on carbon; hydrogen / ethyl acetate / 4 h / 20 °C

With sulfuric acid; platinum on carbon; hydrogen; potassium carbonate; sodium nitrite; In water; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1021/jm300185p

upstream raw materials:

4-aminoindazole

4-hydroxyindazole

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