3-fluoro-4-(hydroxymethyl)phenol

Base Information

• Chemical Name: 3-fluoro-4-(hydroxymethyl)phenol
• CAS No.: 96740-92-0
• Molecular Formula: C7H7FO2
• Molecular Weight: 142.13
• Hs Code.: 2908199090
• Mol file: 96740-92-0.mol

Synonyms:2-fluoro-4-hydroxybenzyl alcohol;methyl 2-fluoro-4-hydroxy-benzoate;2-fluoro-4-hydroxybenzoic acid methyl ester;2-fluoro-4-hyroxybenzoic acid methyl ester;

Chemical Property of 3-fluoro-4-(hydroxymethyl)phenol

Chemical Property:

• PSA: 40.46000
• LogP: 1.02360
• Storage Temp.: Inert atmosphere,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Fluoro-4-(hydroxymethyl)phenol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Fluoro-4-hydroxybenzenemethanol is a reactant used in the synthesis of cyanophenyl(triazolyl)aminomethylphenyl sulfamates as dual aromatase-sulfatase inhibitors.

Technology Process of 3-fluoro-4-(hydroxymethyl)phenol

There total 4 articles about 3-fluoro-4-(hydroxymethyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-fluoro-4-hydroxybenzaldehyde (348-27-6) → 3-fluoro-4-(hydroxymethyl)phenol (96740-92-0)

Guidance literature:

With sodium tetrahydroborate; In methanol; at 20 ℃; for 0.166667h;

DOI:10.1246/cl.2008.436

Reference yield: 90.0%

2-fluoro-4-hydroxybenzoic acid (65145-13-3) → 3-fluoro-4-(hydroxymethyl)phenol (96740-92-0)

Guidance literature:

With Trimethyl borate; dimethylsulfide borane complex; In tetrahydrofuran;

DOI:10.1016/S0040-4039(98)01541-X

Reference yield: 76.0%

methyl 2-fluoro-4-hydroxybenzoate (197507-22-5) → 3-fluoro-4-(hydroxymethyl)phenol (96740-92-0)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 0.75h;

DOI:10.1002/cmdc.201300015

upstream raw materials:

2-fluoro-4-hydroxybenzoic acid

2-fluoro-4-propoxybenzoic acid

2-fluoro-4-hydroxybenzaldehyde

methyl 2-fluoro-4-hydroxybenzoate

Downstream raw materials:

(3-Fluoro-4-hydroxymethyl-phenoxy)-acetic acid ethyl ester

3-fluoro-4-(hydroxymethyl)phenoxyacetic acid

4-benzyloxy-2-fluoro-benzyl alcohol

4-[(2-fluoro-4-hydroxybenzyl)(4H-1,2,4-triazol-4-yl)amino]benzonitrile

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