2,3-DIMETHYLISONICOTINALDEHYDE

Base Information

• Chemical Name: 2,3-DIMETHYLISONICOTINALDEHYDE
• CAS No.: 867141-55-7
• Molecular Formula: C8H9NO
• Molecular Weight: 135.16
• Hs Code.: 2933399090
• Mol file: 867141-55-7.mol

Synonyms:2,3-DIMETHYLISONICOTINALDEHYDE;2,3-DIMETHYLPYRIDINE-4-CARBALDEHYDE;4-METHOXY-2,3-DIMETHYLPYRIDINE

Chemical Property of 2,3-DIMETHYLISONICOTINALDEHYDE

Chemical Property:

• Vapor Pressure: 0.0363mmHg at 25°C
• Boiling Point: 241.3°C at 760 mmHg
• Flash Point: 105.8°C
• PSA: 29.96000
• Density: 1.065g/cm³
• LogP: 1.51090

Purity/Quality:

97% ^*data from raw suppliers

2,3-Dimethylpyridine-4-carbaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,3-DIMETHYLISONICOTINALDEHYDE

There total 1 articles about 2,3-DIMETHYLISONICOTINALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2,3-dimethylpyridin-4-yl)-methanol (867141-54-6) → 2,3-dimethylisonicotinaldehyde (867141-55-7)

Guidance literature:

(2,3-dimethylpyridin-4-yl)-methanol; With 4-methylmorpholine N-oxide; In dichloromethane; at 0 ℃; for 0.166667h; Molecular sieve;

tetrapropylammonium perruthennate; at 20 ℃; for 16h;

Reference yield:

2,3-dimethylisonicotinaldehyde (867141-55-7) + 4-[4-chloro-3-trifluoromethylphenyl]-4-piperidinol (21928-50-7) → 4-(4-chloro-3-trifluoromethylphenyl)-1-(2,3-dimethyl-pyridin-4-ylmethyl)-piperidin-4-ol

Guidance literature:

With Sodium triacetoxy borohydride; acetic acid; In dichloromethane; at 70 ℃;

Reference yield:

1-(4-chloro-3-methoxyphenyl)piperazine (637022-44-7) + 2,3-dimethylisonicotinaldehyde (867141-55-7) + methylmagnesium bromide (75-16-1) → 1-(4-chloro-3-methoxyphenyl)-4-[1-(2,3-dimethylpyridin-4-yl)-ethyl]-piperazine

Guidance literature:

1-(4-chloro-3-methoxyphenyl)piperazine; 2,3-dimethylisonicotinaldehyde; With 1,2,3-Benzotriazole; In ethanol; toluene; at 40 ℃;

methylmagnesium bromide; In tetrahydrofuran; toluene; at 20 ℃; for 2h;

upstream raw materials:

(2,3-dimethylpyridin-4-yl)-methanol

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