[9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA)

Base Information

Chemical Name:[9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA)
CAS No.:1133057-97-2
Molecular Formula:C22H16BNO2
Molecular Weight:337.186
Hs Code.:
Mol file:1133057-97-2.mol

Synonyms:[9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA);B-[9-(1-Naphthalenyl)-9H-carbazol-3-yl]-boronic acid;[9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid;[9-(1-phthalenyl)-9H-carbazol-3-yl]-Boronic acid

Suppliers and Price of [9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of [9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA)

Chemical Property:

Boiling Point:548.4±56.0 °C(Predicted)
PKA:8.82±0.30(Predicted)
PSA：45.39000
Density:1.22±0.1 g/cm3 (20 oC 760 Torr)
LogP:3.61670

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA)

There total 2 articles about [9-(1-naphthalenyl)-9H-carbazol-3-yl]-Boronic acid(1NCBA) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 934545-83-2
3-bromo-9-(naphthalen-1-yl)-9H-carbazole

: 121-43-7,63156-11-6
Trimethyl borate

: 1133057-97-2
(9-(naphthalen-1-yl)-9H-carbazol-3-yl)boronic acid

Guidance literature:: 3-bromo-9-(naphthalen-1-yl)-9H-carbazole; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 2h;

Trimethyl borate; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 19h;

With hydrogenchloride; water; In tetrahydrofuran; hexane; at 20 ℃; for 4h;

Reference yield:

: 1133057-97-2
(9-(naphthalen-1-yl)-9H-carbazol-3-yl)boronic acid

Guidance literature:: With n-butyllithium; In diethyl ether; hexane; at -78 ℃; for 0.5h;

In diethyl ether; hexane; at -78 - 20 ℃;

With hydrogenchloride;

Reference yield: 68.0%

: 1133057-97-2
(9-(naphthalen-1-yl)-9H-carbazol-3-yl)boronic acid

: C₂₆H₁₄BrN₅

: C₄₈H₂₈N₆

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In water; toluene; for 12h; Inert atmosphere; Reflux;