p-(Fluorophenyl)triethoxysilane

Base Information

• Chemical Name: p-(Fluorophenyl)triethoxysilane
• CAS No.: 33715-53-6
• Molecular Formula: C12H19FO3Si
• Molecular Weight: 258.365
• Mol file: 33715-53-6.mol

Synonyms:triethoxy(4-fluorophenyl)-silane;Silane, triethoxy(4-fluorophenyl)-;p-Fluorphenyltriethoxysilan;

Chemical Property of p-(Fluorophenyl)triethoxysilane

Chemical Property:

• PSA: 27.69000
• LogP: 2.08110

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-(Fluorophenyl)triethoxysilane

There total 3 articles about p-(Fluorophenyl)triethoxysilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

tetraethoxy orthosilicate (78-10-4) + 1-Bromo-4-fluorobenzene (460-00-4) → triethoxy(4-fluorophenyl)silane (33715-53-6)

Guidance literature:

With magnesium; In tetrahydrofuran; at 70 ℃; for 12h; Schlenk technique; Inert atmosphere;

DOI:10.1002/asia.201901155

Reference yield:

tetraethoxy orthosilicate (78-10-4) + 4-flourophenylmagnesium bromide (352-13-6) → triethoxy(4-fluorophenyl)silane (33715-53-6)

Guidance literature:

In tetrahydrofuran;

DOI:10.1016/S0022-328X(03)00469-8

Reference yield:

→ triethoxy(4-fluorophenyl)silane (33715-53-6)

Guidance literature:

entspr. Aryltrichlorsilan, A.;

DOI:10.1021/ja00824a011

upstream raw materials:

tetraethoxy orthosilicate

4-flourophenylmagnesium bromide

1-Bromo-4-fluorobenzene

Downstream raw materials:

2-(4-fluorophenyl)benzoxazole

dodecyl 4-fluorobenzenethioate

diethyl (4-fluorophenyl)phosphonate

N,N-dibenzyl-4-fluorobenzamide