5-Bromo-2-((tert-Butyldimethylsilyloxy)methyl)-3-methoxypyridine

Base Information

• Chemical Name: 5-Bromo-2-((tert-Butyldimethylsilyloxy)methyl)-3-methoxypyridine
• CAS No.: 1138443-85-2
• Molecular Formula: C13H22BrNO2Si
• Molecular Weight: 332.31
• Hs Code.: 2933399090

Synonyms:(5-bromo-3-methoxypyridin-2-yl)methoxy-tert-butyl-dimethylsilane;

Chemical Property of 5-Bromo-2-((tert-Butyldimethylsilyloxy)methyl)-3-methoxypyridine

Chemical Property:

• PSA: 31.35000
• LogP: 4.37450

Purity/Quality:

97% ^*data from raw suppliers

5-Bromo-2-((tert-butyldimethylsilyloxy)methyl)-3-methoxypyridine ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xn
• Hazard Codes: Xn
• Statements: 22

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-Bromo-2-((tert-Butyldimethylsilyloxy)methyl)-3-methoxypyridine

There total 1 articles about 5-Bromo-2-((tert-Butyldimethylsilyloxy)methyl)-3-methoxypyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(5-bromo-3-methoxypyridin-2-yl)methanol (1087659-32-2) + tert-butyldimethylsilyl chloride (18162-48-6) → 5-bromo-2-(((tert-butyldimethylsilyl)oxy)methyl)-3-methoxypyridine (1138443-85-2)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 20 ℃; for 3h;

Reference yield:

5-bromo-2-(((tert-butyldimethylsilyl)oxy)methyl)-3-methoxypyridine (1138443-85-2) + (2-((benzyloxy)carbonyl)-2-azaspiro[3.3]heptan-6-yl)zinc(II) iodide → C21H24N2O4

Guidance literature:

5-bromo-2-(((tert-butyldimethylsilyl)oxy)methyl)-3-methoxypyridine; (2-((benzyloxy)carbonyl)-2-azaspiro[3.3]heptan-6-yl)zinc(II) iodide; With copper(l) iodide; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In N,N-dimethyl-formamide; at 70 ℃; Inert atmosphere;

With triethylamine tris(hydrogen fluoride); In N,N-dimethyl-formamide;

upstream raw materials:

(5-bromo-3-methoxypyridin-2-yl)methanol

tert-butyldimethylsilyl chloride

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