2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde

Base Information

Chemical Name:2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde
CAS No.:1053265-66-9
Molecular Formula:C9H13BrO
Molecular Weight:217.106
Hs Code.:
Mol file:1053265-66-9.mol

Synonyms:2-bromo-5,5-dimethylcyclohexene-1-carbaldehyde; 2-bromo-5,5-dimethylcyclohex-1-enecarbaldehyde; 2-bromo-5,5-dimethylcyclohex-1-ene-1-carbaldehyde; QC-9191

Suppliers and Price of 2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
2-Bromo-5,5-dimethylcyclohex-1-enecarbaldehyde 95%
5g
$ 1074.00

Total 9 raw suppliers

Chemical Property of 2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde

Chemical Property:

Boiling Point:240.6±40.0 °C(Predicted)
PSA：17.07000
Density:1.399±0.06 g/cm3(Predicted)
LogP:3.04440

Purity/Quality:

98%min ^*data from raw suppliers

2-Bromo-5,5-dimethylcyclohex-1-enecarbaldehyde 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde

There total 2 articles about 2-BroMo-5,5-diMethylcyclohex-1-enecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4255-62-3
4,4-dimethylcyclohexane-1-one

: 1053265-66-9
2-bromo-5,5'-bis-methylcyclohex-1-enylcarbaldehyde

Guidance literature:: With phosphorus tribromide; In N,N-dimethyl-formamide; at 0 - 60 ℃;

Reference yield:

: 1073-13-8
4,4-dimethylcyclohexenone

: 1053265-66-9
2-bromo-5,5'-bis-methylcyclohex-1-enylcarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogen / 5%-palladium/activated carbon / ethyl acetate / 2 h / 20 °C / 760.05 Torr

2.1: phosphorus tribromide / dichloromethane / 0.5 h / 0 - 20 °C

2.2: 4 h / 0 - 20 °C

With hydrogen; phosphorus tribromide; 5%-palladium/activated carbon; In dichloromethane; ethyl acetate;

Reference yield: 81.0%

: 1053265-66-9
2-bromo-5,5'-bis-methylcyclohex-1-enylcarbaldehyde

: C₉H₁₃BrO₂

Guidance literature:: With sodium chlorite; potassium dihydrogenphosphate; dihydrogen peroxide; In acetonitrile; at 0 - 20 ℃; for 5h;
DOI:10.1039/d1ob02106k