ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

Base Information

Chemical Name:ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate
CAS No.:1065604-58-1
Molecular Formula:C₂₂H₃₁BrN₂O₂
Molecular Weight:435.404
Hs Code.:

Synonyms:ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

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Chemical Property of ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

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Technology Process of ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

There total 3 articles about ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1053265-66-9
2-bromo-5,5'-bis-methylcyclohex-1-enylcarbaldehyde

: 80518-57-6
ethyl 4-(piperazin-1-yl)benzoate

: 1065604-58-1
ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

Guidance literature:: With sodium cyanoborohydride; acetic acid; In ethanol; at 20 ℃; for 15h; pH=5; Inert atmosphere;
DOI:10.1021/jm800669s

Reference yield:

: 451-46-7
4-fluorobenzoic acid ethyl ester

: 1065604-58-1
ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyl sulfoxide / 120 °C

2: acetic acid; sodium tris(acetoxy)borohydride / ethanol / 20 °C / pH 5

With sodium tris(acetoxy)borohydride; acetic acid; In ethanol; dimethyl sulfoxide;

Reference yield:

: 4255-62-3
4,4-dimethylcyclohexane-1-one

: 1065604-58-1
ethyl 4-(4-((2-bromo-5,5-dimethylcyclohex-1-enyl)methyl)piperazin-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus tribromide / chloroform / 2 h / 0 - 70 °C

2: acetic acid; sodium tris(acetoxy)borohydride / ethanol / 20 °C / pH 5

With phosphorus tribromide; sodium tris(acetoxy)borohydride; acetic acid; In ethanol; chloroform;