FMOC-4-Amino-D-phenylalanine

Base Information

• Chemical Name: FMOC-4-Amino-D-phenylalanine
• CAS No.: 324017-21-2
• Molecular Formula: C24H22N2O4
• Molecular Weight: 402.44200
• Hs Code.: 2924299090
• Mol file: 324017-21-2.mol

Synonyms:Fmoc-4-amino-D-phenylalanine;4-Amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-D-phenylalanine;4-Amino-D-phenylalanine,N-FMOC protected;

Chemical Property of FMOC-4-Amino-D-phenylalanine

Chemical Property:

• Boiling Point: 671.5±55.0 °C(Predicted)
• PKA: 3.63±0.10(Predicted)
• PSA: 101.65000
• Density: 1.316±0.06 g/cm3(Predicted)
• LogP: 4.77530
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

97% ^*data from raw suppliers

4-Amino-D-phenylalanine, N-Fmoc protected ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of FMOC-4-Amino-D-phenylalanine

There total 14 articles about FMOC-4-Amino-D-phenylalanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-α-FMOC-4-nitro-L-phenylalanine (95753-55-2,177966-63-1) → 4-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-phenylalanine (95753-56-3,324017-21-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 1h;

DOI:10.1016/S0960-894X(97)00088-7

Reference yield:

N-α-FMOC-4-nitro-L-phenylalanine (95753-55-2,177966-63-1) → isopropyl ether of N-[(9H-fluoren-9-ylmethoxy)carbonyl]-4-amino-L-phenylalanine + 4-amino-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-phenylalanine (95753-56-3,324017-21-2)

Guidance literature:

With hydrogenchloride; zinc; In water; isopropyl alcohol;

DOI:10.1134/S1070428016110221

Reference yield:

(2R)-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-3-(4-nitrophenyl)propionic acid (177966-63-1) → isopropyl ether of N-[(9H-fluoren-9-ylmethoxy)carbonyl]-4-amino-D-phenylalanine + (2R)-2-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}-3-(4-aminophenyl)propionic acid (324017-21-2)

Guidance literature:

With hydrogenchloride; zinc; In water; isopropyl alcohol;

DOI:10.1134/S1070428016110221

upstream raw materials:

N-α-FMOC-4-nitro-L-phenylalanine

4-amino-L-phenylalanine

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

4-nitro-3-phenyl-L-alanine

Downstream raw materials:

N-Fmoc-L-p-aminophenylalanine methyl ester hydrochloride

(S)-tert-butyl (4-(2-amino-3-(methoxy(methyl)amino)-3-oxopropyl)phenyl)carbamate

(S)-tert-butyl (4-(3-(methoxy(methyl)amino)-3-oxo-2-(tritylamino)propyl)phenyl)carbamate

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