3-Bromo-5-Iodobenzonitrile

Base Information

• Chemical Name: 3-Bromo-5-Iodobenzonitrile
• CAS No.: 289039-21-0
• Molecular Formula: C₇H₃BrIN
• Molecular Weight: 307.916
• Hs Code.: 2926907090
• Mol file: 289039-21-0.mol

Synonyms:3-BROMO-5-IODOBENZONITRILE

Chemical Property of 3-Bromo-5-Iodobenzonitrile

Chemical Property:

• PSA: 23.79000
• Density: 2.31
• LogP: 2.92538
• Storage Temp.: Keep in dark place,Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

3-Bromo-5-iodobenzonitrile tech ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Bromo-5-Iodobenzonitrile

There total 4 articles about 3-Bromo-5-Iodobenzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-bromo-5-iodo-benzaldehyde (188813-09-4) → 3-bromo-5-iodobenzonitrile (289039-21-0)

Guidance literature:

With ammonium hydroxide; iodine; In tetrahydrofuran;

Reference yield:

3-bromo-5-iodo-benzoic acid (188815-32-9) → 3-bromo-5-iodobenzonitrile (289039-21-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: thionyl chloride / 2 h / 81 °C

2.1: ammonium hydroxide / 3 h / 20 °C

2.2: 18 h / Reflux

With ammonium hydroxide; thionyl chloride;

DOI:10.1021/acsmedchemlett.9b00495

Reference yield:

3-bromo-5-iodobenzoyl chloride (810681-06-2) → 3-bromo-5-iodobenzonitrile (289039-21-0)

Guidance literature:

3-bromo-5-iodobenzoyl chloride; With ammonium hydroxide; at 20 ℃; for 3h;

With thionyl chloride; for 18h; Reflux;

DOI:10.1021/acsmedchemlett.9b00495

upstream raw materials:

3-bromo-5-iodo-benzoic acid

3-bromo-5-iodobenzoyl chloride

1-bromo-3-(hydroxymethyl)-5-iodobenzene

3-bromo-5-iodo-benzaldehyde

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