Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate

Base Information

• Chemical Name: Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate
• CAS No.: 1095822-21-1
• Molecular Formula: C8H8Cl2N2O2
• Molecular Weight: 235.07
• Hs Code.: 2933599090
• Mol file: 1095822-21-1.mol

Synonyms:Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate;Ethyl (4,6-dichloro-5-pyrimidinyl)acetate

Chemical Property of Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate

Chemical Property:

• PSA: 52.08000
• LogP: 1.88900

Purity/Quality:

97% ^*data from raw suppliers

Ethyl 2-(4,6-dichloro-5-pyrimidyl)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate

There total 1 articles about Ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.5%

ethyl 2-(4,6-dihydroxypyrimidin-5-yl)acetate (1095822-20-0) → ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate (1095822-21-1)

Guidance literature:

With triethylamine; trichlorophosphate; In toluene; at 110 - 115 ℃; for 3h;

Reference yield: 71.0%

ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate (1095822-21-1) + 2,4,6-trimethoxybenzylamine (77648-20-5) → C18H22ClN3O5 (1095822-22-2)

Guidance literature:

With triethylamine; In ethanol; at 80 ℃; for 4h;

Reference yield:

ethyl 2-(4,6-dichloropyrimidin-5-yl)acetate (1095822-21-1) + 2,4-Dimethoxybenzylamine (20781-20-8) → C17H20ClN3O4

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 60 - 65 ℃; for 3h;

upstream raw materials:

ethyl 2-(4,6-dihydroxypyrimidin-5-yl)acetate

Downstream raw materials:

C₁₈H₂₂ClN₃O₅

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