N-(6-BroMoiMidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetaMide

Base Information

• Chemical Name: N-(6-BroMoiMidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetaMide
• CAS No.: 504413-35-8
• Molecular Formula: C9H5BrF3N3O
• Molecular Weight: 308.057
• Hs Code.: 2933990090
• Mol file: 504413-35-8.mol

Synonyms:N-(6-bromoimidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide;

Chemical Property of N-(6-BroMoiMidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetaMide

Chemical Property:

• PSA: 49.89000
• LogP: 3.24710
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

N-(6-BromoH-imidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide ^*data from reagent suppliers

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MSDS Files:

SDS file from LookChem

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Technology Process of N-(6-BroMoiMidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetaMide

There total 7 articles about N-(6-BroMoiMidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-[5-bromo-2-{[(4-methylphenyl)sulfonyl]imino}pyridin-1(2H)-yl]acetamide (1005785-49-8) + trifluoroacetic anhydride (407-25-0) → N-(6-bromoimidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide (504413-35-8)

Guidance literature:

In 1,2-dichloro-ethane; at 60 ℃; for 2h;

Reference yield: 50.0%

2-[(2E)-5-bromo-2-(p-tolylsulfonylimino)-1-pyridyl]acetamide + trifluoroacetic anhydride (407-25-0) → N-(6-bromoimidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide (504413-35-8)

Guidance literature:

In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield: 38.0%

2,2,2-trifluoro-N-(6-iodoimidazo[1,2-a]pyridin-2-yl)acetamide (209971-49-3) → 2,2,2-trifluoro-N-(imidazo[1,2-a]pyridin-2-yl)acetamide + N-(6-bromoimidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide (504413-35-8)

Guidance literature:

With bromocyane; isopropylmagnesium chloride; In tetrahydrofuran; at -40 - 0 ℃; for 3h;

DOI:10.1016/S0040-4039(02)02278-5

upstream raw materials:

2,2,2-trifluoro-N-(6-iodoimidazo[1,2-a]pyridin-2-yl)acetamide

(Z)-2-(5-bromo-2-(tosylimino)pyridin-1(2H)-yl)acetamide

trifluoroacetic anhydride

2-[5-bromo-2-{[(4-methylphenyl)sulfonyl]imino}pyridin-1(2H)-yl]acetamide

Downstream raw materials:

2,2,2-trifluoro-N-{6-[3-(methylsulfonyl)phenyl]imidazo[1,2-a]pyridin-2-yl}acetamide

N-(6-{3-[(ethylamino)sulfonyl]phenyl}imidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide

N-(6-bromoimidazo[1,2-a]pyridin-2-yl)acetamide

N-(6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)imidazo[1,2-a]pyridine-2-yl)acetamide

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