(E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide

Base Information

• Chemical Name: (E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide
• CAS No.: 1005785-49-8
• Molecular Formula: C14H14BrN3O3S
• Molecular Weight: 384.253
• Mol file: 1005785-49-8.mol

Synonyms:(E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide;2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide

Chemical Property of (E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide

Chemical Property:

• PSA: 102.90000
• LogP: 3.11500
• Storage Temp.: 2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

(E)-2-(5-Bromo-2-(tosylimino)pyridin-1(2H)-yl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide

There total 3 articles about (E)-2-(5-BroMo-2-(tosyliMino)pyridin-1(2H)-yl)acetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

iodacetamide (144-48-9) + N-(5-bromopyridin-2(1H)-ylidene)-4-methylbenzenesulfonamide (207801-52-3) → 2-[5-bromo-2-{[(4-methylphenyl)sulfonyl]imino}pyridin-1(2H)-yl]acetamide (1005785-49-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 15h; Product distribution / selectivity;

Reference yield: 87.0%

bromo-acetic acid amide (683-57-8) + N-(5-bromopyridin-2-yl)-4-methylbenzenesulfonamide (207801-52-3) → 2-[5-bromo-2-{[(4-methylphenyl)sulfonyl]imino}pyridin-1(2H)-yl]acetamide (1005785-49-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25 ℃; for 24h; Product distribution / selectivity;

Reference yield: 82.0%

N-(5-bromopyridin-2-yl)-4-methylbenzenesulfonamide (207801-52-3) + Chloroacetamide (79-07-2) → 2-[5-bromo-2-{[(4-methylphenyl)sulfonyl]imino}pyridin-1(2H)-yl]acetamide (1005785-49-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 80 ℃; for 48h;

upstream raw materials:

bromo-acetic acid amide

N-(5-bromopyridin-2-yl)-4-methylbenzenesulfonamide

iodacetamide

N-(5-bromopyridin-2(1H)-ylidene)-4-methylbenzenesulfonamide

Downstream raw materials:

N-(6-bromoimidazo[1,2-a]pyridin-2-yl)acetamide

N-(6-bromoimidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide

N-(6-{3-[(ethylamino)sulfonyl]phenyl}imidazo[1,2-a]pyridin-2-yl)-2,2,2-trifluoroacetamide

2,2,2-trifluoro-N-{6-[3-(methylsulfonyl)phenyl]imidazo[1,2-a]pyridin-2-yl}acetamide

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