Imidazo[1,5-a]pyrimidine-6-carboxylic acid, 2,4-dimethyl-, ethyl ester

Base Information

• Chemical Name: Imidazo[1,5-a]pyrimidine-6-carboxylic acid, 2,4-dimethyl-, ethyl ester
• CAS No.: 959015-28-2
• Molecular Formula: C11H13N3O2
• Molecular Weight: 219.24000
• Mol file: 959015-28-2.mol

Synonyms:

Chemical Property of Imidazo[1,5-a]pyrimidine-6-carboxylic acid, 2,4-dimethyl-, ethyl ester

Chemical Property:

• PSA: 56.49000
• LogP: 1.52280

Purity/Quality:

98% ^*data from raw suppliers

2,4-dimethyl-Imidazo[1,5-a]pyrimidine-6-carboxylicacidethylester 97.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Imidazo[1,5-a]pyrimidine-6-carboxylic acid, 2,4-dimethyl-, ethyl ester

There total 1 articles about Imidazo[1,5-a]pyrimidine-6-carboxylic acid, 2,4-dimethyl-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

ethyl 5-nitro-1H-imidazole-2-carboxylate (865998-46-5) + acetylacetone (123-54-6,81235-32-7) → C11H13N3O2 (959015-28-2)

Guidance literature:

ethyl 5-nitro-1H-imidazole-2-carboxylate; With 5% Pd(II)/C(eggshell); hydrogen; In methanol; for 1h; under 760.051 Torr; Inert atmosphere;

acetylacetone; With acetic acid; In methanol; Reflux;

DOI:10.2174/157017809787893000

upstream raw materials:

ethyl 5-nitro-1H-imidazole-2-carboxylate

acetylacetone

Refernces