4-Amino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate

Base Information

• Chemical Name: 4-Amino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate
• CAS No.: 1032350-07-4
• Molecular Formula: C₂HF₃O₂*C₆H₅ClN₂O
• Molecular Weight: 270.595
• Hs Code.: 2933399090
• Mol file: 1032350-07-4.mol

Synonyms:4-AMino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate;4-Amino-2-chloro-3-pyridinecarboxaldehyde 2,2,2-trifluoroacetate

Chemical Property of 4-Amino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate

Chemical Property:

• PSA: 93.28000
• LogP: 2.34420
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

4-Amino-2-chloronicotinaldehyde2,2,2-trifluoroacetate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Amino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate

There total 1 articles about 4-Amino-2-chloronicotinaldehyde 2,2,2-trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl (2-chloro-3-formylpyridin-4-yl)carbamate (893423-62-6) + trifluoroacetic acid (76-05-1) → 4-amino-2-chloronicotinaldehyde trifluoroacetate (1032350-07-4)

Guidance literature:

In dichloromethane; at 25 - 35 ℃;

Reference yield:

tert-butyl 1-(4-(2-phenylacetyl)phenyl)cyclobutylcarbamate (1032349-98-6) + 4-amino-2-chloronicotinaldehyde trifluoroacetate (1032350-07-4) → tert-butyl {1-[4-(5-chloro-3-phenyl-1,6-naphthyrindin-2-yl)phenyl]cyclobutyl}carbamate (1032349-99-7)

Guidance literature:

With potassium hydroxide; In water; isopropyl alcohol; at 24 ℃; for 1h; Product distribution / selectivity;

upstream raw materials:

tert-butyl (2-chloro-3-formylpyridin-4-yl)carbamate

trifluoroacetic acid

Downstream raw materials:

tert-butyl {1-[4-(5-chloro-3-phenyl-1,6-naphthyrindin-2-yl)phenyl]cyclobutyl}carbamate

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