Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester

Base Information

Chemical Name:Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester
CAS No.:942145-77-9
Molecular Formula:C18H22N2O2
Molecular Weight:298.385
Hs Code.:2933990090
Mol file:942145-77-9.mol

Synonyms:Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester;1,2,3,6-TETRAHYDRO-1,1-DIMETHYL-AZEPINO[4,5-B]INDOLE-5-CARBOXYLIC ACID 1-METHYLETHYL ESTER

Suppliers and Price of Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Isopropyl1,1-dimethyl-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate 95+%
1g
$ 772.00

ChemScene
Azepino[4,5-b]indole-5-carboxylicacid,1,2,3,6-tetrahydro-1,1-dimethyl-,1-methylethylester
1g
$ 2090.00

American Custom Chemicals Corporation
ISOPROPYL-1,1-DIMETHYL-1,2,3,6-TETRAHYDROAZEPINO[4,5-B]INDOLE-5-CARBOXYLATE 95.00%
5MG
$ 497.53

Alichem
Isopropyl1,1-dimethyl-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate
1g
$ 659.40

Total 10 raw suppliers

Chemical Property of Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester

Chemical Property:

Vapor Pressure:7.81E-10mmHg at 25°C
Boiling Point:492.3°C at 760 mmHg
PKA:18.26±0.60(Predicted)
Flash Point:251.5°C
PSA：54.12000
Density:1.133g/cm³
LogP:3.67000

Purity/Quality:

98%Min ^*data from raw suppliers

Isopropyl1,1-dimethyl-1,2,3,6-tetrahydroazepino[4,5-b]indole-5-carboxylate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester

There total 2 articles about Azepino[4,5-b]indole-5-carboxylic acid, 1,2,3,6-tetrahydro-1,1-dimethyl-, 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1227748-44-8
isopropyl 1-(bromomethyl)-4,4-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-1-carboxylate

: 1227748-49-3
isopropyl 1-(chloromethyl)-4,4-dimethyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-1-carboxylate

: 942145-77-9
isopropyl 1,1-dimethyl-1,2,3,6-tetrahydro-azepino[4,5-b]indole-5-carboxylate

Guidance literature:: With pyridine; dmap; at 20 ℃; Heating / reflux;

Reference yield:

: 56417-63-1
iso-propyl 3-bromo-2-oxopropanoate

: 15467-31-9
2-(1H-indol-3-yl)-2-methylpropane-1-amine

: 942145-77-9
isopropyl 1,1-dimethyl-1,2,3,6-tetrahydro-azepino[4,5-b]indole-5-carboxylate

Guidance literature:: 2-(1H-indol-3-yl)-2-methylpropane-1-amine; With hydrogenchloride; In 1,4-dioxane; ethanol; charcoal;

iso-propyl 3-bromo-2-oxopropanoate; In 1,4-dioxane; ethanol; Reflux; charcoal;

With pyridine; at 100 ℃; charcoal;
DOI:10.1021/jm8014124