Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III)

Base Information

• Chemical Name: Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III)
• CAS No.: 344796-05-0
• Molecular Formula: C35H27IrN2O4
• Molecular Weight: 731.83

Synonyms:Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III);Ir(ppo)2(acac)

Chemical Property of Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III)

Chemical Property:

• PSA: 92.19000
• LogP: 8.21810

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III)

There total 1 articles about Bis(2,5-diphenyloxazole-C2,N')(acetylacetonato)iridium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

(2,4-diphenyloxazolato-1,3-N,C2')2Ir(μ-Cl)2Ir(2,4-diphenyloxazolato-1,3-N,C2')2 + acetylacetone (123-54-6,81235-32-7) → iridium(III) bis(2,4-diphenyloxazolato-1,3-N,C2')(acetylacetonate) (344796-05-0)

Guidance literature:

With sodium carbonate; In 2-ethoxy-ethanol; byproducts: HCl; under inert atmosphere; mixt. of Ir complex and ligand (molar ratio 1:2.5) and Na2CO3 heated under reflux in 2-ethoxyethanol for 12-15 h; cooledto room temp.; filtered; ppt. washed with water, hexane and ether; purified by flash chromy. (silica column, CH2Cl2); solvent evapd.; dried; elem. anal.;

DOI:10.1021/ja003693s

upstream raw materials:

acetylacetone

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