β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1

Base Information

• Chemical Name: β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1
• CAS No.: 139994-47-1
• Molecular Formula: C38H28N2
• Molecular Weight: 512.64
• Mol file: 139994-47-1.mol

Synonyms:β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1;N,N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1,4-diaMine

Chemical Property of β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1

Chemical Property:

• Melting Point: 200℃
• PSA: 0.00000
• LogP: 0.00000

Purity/Quality:

97% ^*data from raw suppliers

N,N''-Di(Naphthalen-2-Yl)-N,N''-Diphenylbenzene-1,4-Diamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: N,N''-Di(Naphthalen-2-Yl)-N,N''-Diphenylbenzene-1,4-Diamine is a component of organic light emitting devices.

Technology Process of β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1

There total 2 articles about β- NPP , N, N'-di(naphthalen-2-yl)-N,N'-diphenylbenzene-1 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bromoiodobenzene (589-87-7) + di-p-tolylamine (620-93-9) → N1,N1,N4,N4-di(naphthalen-2-yl)-N1,N4-diphenylbenzene-1,4-diamine (139994-47-1) + 4-bromo-N,N-di-p-tolylaniline (58047-42-0)

Guidance literature:

With copper(l) iodide; sodium t-butanolate; In tetrahydrofuran; at 100 ℃; for 12h; Overall yield = 92 %; chemoselective reaction; Catalytic behavior; Inert atmosphere;

DOI:10.1016/j.tet.2015.01.028

Reference yield:

1,4-bromoiodobenzene (589-87-7) + N-Phenyl-2-naphthylamine (135-88-6,84420-28-0) → N1,N1,N4,N4-di(naphthalen-2-yl)-N1,N4-diphenylbenzene-1,4-diamine (139994-47-1) + 4-bromo-N,N-di-p-tolylaniline (58047-42-0)

Guidance literature:

With copper(l) iodide; sodium t-butanolate; In tetrahydrofuran; at 60 ℃; for 12h; Overall yield = 95 %; chemoselective reaction; Catalytic behavior; Inert atmosphere;

DOI:10.1016/j.tet.2015.01.028

upstream raw materials:

1,4-bromoiodobenzene

di-p-tolylamine

N-Phenyl-2-naphthylamine

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