TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Base Information

Chemical Name:TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane
CAS No.:937082-80-9
Molecular Formula:C₄₃H₃₂Si
Molecular Weight:576.813
Hs Code.:
Mol file:937082-80-9.mol

Synonyms:TPSIF;9-Phenyl-9-[4-(triphenylsilyl)phenyl]-9H-fluorene;Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane;TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Suppliers and Price of TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Chemical Property:

Purity/Quality:: 98%Min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

There total 3 articles about TPSiF , Triphenyl(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 937082-81-0
9-(4-bromophenyl)-9-phenyl-9H-fluorene

: 76-86-8
Triphenylsilyl chloride

: 937082-80-9
triphenyl-(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Guidance literature:: 9-(4-bromophenyl)-9-phenyl-9H-fluorene; With n-butyllithium; In diethyl ether; hexane; at -78 - 0 ℃;

Triphenylsilyl chloride; In diethyl ether; hexane; for 4h; Further stages.; Heating;
DOI:10.1039/b616043c

Reference yield:

: 79653-80-8
9-(4-bromophenyl)-9H-fluoren-9-ol

: 937082-80-9
triphenyl-(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 28 percent / CF₃SO₃H / 4 h / Heating

2.1: n-BuLi / hexane; diethyl ether / -78 - 0 °C

2.2: 74 percent / diethyl ether; hexane / 4 h / Heating

With n-butyllithium; trifluorormethanesulfonic acid; In diethyl ether; hexane;
DOI:10.1039/b616043c

Reference yield:

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 937082-80-9
triphenyl-(4-(9-phenyl-9H-fluoren-9-yl)phenyl)silane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 28 percent / CF₃SO₃H / 4 h / Heating

2.1: n-BuLi / hexane; diethyl ether / -78 - 0 °C

2.2: 74 percent / diethyl ether; hexane / 4 h / Heating

With n-butyllithium; trifluorormethanesulfonic acid; In diethyl ether; hexane;
DOI:10.1039/b616043c