9-(N,N-diMethylaMinoMethyl)anthracene

Base Information

• Chemical Name: 9-(N,N-diMethylaMinoMethyl)anthracene
• CAS No.: 42758-92-9
• Molecular Formula: C17H17N
• Molecular Weight: 235.329
• Mol file: 42758-92-9.mol

Synonyms:[9]anthrylmethyl-dimethyl-amine;9-[(dimethylamino)methyl]anthracene;9-N-dimethylaminomethylanthracene;[9]Anthrylmethyl-dimethyl-amin;9-(N,N-dimethylaminomethyl)anthracene;

Chemical Property of 9-(N,N-diMethylaMinoMethyl)anthracene

Chemical Property:

• Melting Point: 75-77 °C(Solv: ethanol (64-17-5))
• Boiling Point: 375.8±11.0 °C(Predicted)
• PKA: 8.80±0.28(Predicted)
• PSA: 3.24000
• Density: 1.098±0.06 g/cm3(Predicted)
• LogP: 4.05460

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 9-(N,N-diMethylaMinoMethyl)anthracene

There total 5 articles about 9-(N,N-diMethylaMinoMethyl)anthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

N,N,N',N'-tetramethyl-6,13-dihydro-7,12[1',2']-benzeno-6,13-ethenobenzo[5,6]cycloocta[1,2b]naphthalene-5,12(7H)-dimethanamine → (anthracen-9-yl)-N,N-dimethylmethanamine (42758-92-9)

Guidance literature:

In dimethylsulfoxide-d6; at 100 ℃; for 0.5h;

DOI:10.1021/jo060315i

Reference yield: 91.0%

N,N-dimethyl-formamide (68-12-2,33513-42-7) + 9-anthracene aldehyde (642-31-9) → (anthracen-9-yl)-N,N-dimethylmethanamine (42758-92-9)

Guidance literature:

With trifluorormethanesulfonic acid; water; at 150 ℃; for 8h; Inert atmosphere;

DOI:10.1039/d0cc02955f

Reference yield:

N,N-dimethylammonium chloride (506-59-2) + 9-anthracene aldehyde (642-31-9) → (anthracen-9-yl)-N,N-dimethylmethanamine (42758-92-9)

Guidance literature:

N,N-dimethylammonium chloride; 9-anthracene aldehyde; With titanium(IV) isopropylate; triethylamine; In ethanol; at 25 ℃; for 10h;

With sodium tetrahydroborate; In ethanol; at 25 ℃; for 10h;

DOI:10.1021/acs.orglett.9b02820

upstream raw materials:

N,N-dimethyl-formamide

9-anthracene aldehyde

N,N-dimethylammonium chloride

Downstream raw materials:

(anthracen-9-ylmethyl)(triphenyl)phosphonium iodide

5,6,11,12-tetrahydro-4b,12<1',2'>:6,10b<1,2>-dibenzenochrysene

1,2,7,8-tetrahydro-2a,7[1',2']:8,12b[1'',2'']-dibezenodibenzo[a,e]cyclobuta[c]cyclooctene

9,10-phenanthrenequinone