[(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI)

Base Information

Chemical Name:[(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI)
CAS No.:307531-87-9
Molecular Formula:C25H23N2O3P
Molecular Weight:430.443
Hs Code.:
Mol file:307531-87-9.mol

Synonyms:[(6-Methyl-pyridin-3-yl)-phenylamino-methyl]-phosphonic acid diphenyl ester;

Suppliers and Price of [(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of [(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI)

Chemical Property:

Melting Point:135 - 137 °C
PSA：70.26000
LogP:6.92480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI)

There total 5 articles about [(6-Methyl-3-pyridinyl)(phenylamino)methyl]-, diphenyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5470-70-2
Methyl 6-methylnicotinate

: 307531-87-9
1-(6-methyl-3-pyridinyl)-1-(aminophenyl)methanodiphenylphosphonic acid

Guidance literature:: Multi-step reaction with 4 steps

1: i-PrMgCl / toluene; tetrahydrofuran / 0.5 h / -10 °C

2: DIBAL-H / toluene / 0.5 h / -20 - -5 °C

3: 46.5 g / isopropyl acetate / 60 °C

4: 46.5 g / isopropyl acetate / 60 - 65 °C

With isopropylmagnesium chloride; diisobutylaluminium hydride; In tetrahydrofuran; Isopropyl acetate; toluene;
DOI:10.1021/jo000870z

Reference yield:

: 221615-71-0
N-methoxy-N-methyl-6-methylnicotinamide

: 307531-87-9
1-(6-methyl-3-pyridinyl)-1-(aminophenyl)methanodiphenylphosphonic acid

Guidance literature:: Multi-step reaction with 3 steps

1: DIBAL-H / toluene / 0.5 h / -20 - -5 °C

2: 46.5 g / isopropyl acetate / 60 °C

3: 46.5 g / isopropyl acetate / 60 - 65 °C

With diisobutylaluminium hydride; In Isopropyl acetate; toluene;
DOI:10.1021/jo000870z

Reference yield:

: 62-53-3
aniline

: 307531-87-9
1-(6-methyl-3-pyridinyl)-1-(aminophenyl)methanodiphenylphosphonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 46.5 g / isopropyl acetate / 60 °C

2: 46.5 g / isopropyl acetate / 60 - 65 °C

In Isopropyl acetate;
DOI:10.1021/jo000870z