N-Succinimidyl 4-(2-pyridyldithio)butanoate

Base Information

Chemical Name:N-Succinimidyl 4-(2-pyridyldithio)butanoate
CAS No.:115088-06-7
Molecular Formula:C13H14N2O4S2
Molecular Weight:326.39
Hs Code.:29251900
European Community (EC) Number:634-558-7
UNII:FAX2C2TAW1
DSSTox Substance ID:DTXSID101347476
Mol file:115088-06-7.mol

Synonyms:N-succinimidyl-3-(2-pyridyldithio)butyrate;SPDB

Suppliers and Price of N-Succinimidyl 4-(2-pyridyldithio)butanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

SynChem
4-(Pyridin-2-yldisulfanyl)butyric acid N-Hydroxysuccinimide ester 90+%
1 g
$ 1950.00

SynChem
4-(Pyridin-2-yldisulfanyl)butyric acid N-Hydroxysuccinimide ester 90+%
250 mg
$ 750.00

DC Chemicals
SPDB >98%
100 mg
$ 250.00

DC Chemicals
SPDB >98%
1 g
$ 1000.00

Crysdot
SPDB 98+%
5mg
$ 69.00

Crysdot
SPDB 98+%
50mg
$ 315.00

Crysdot
SPDB 98+%
100mg
$ 455.00

Crysdot
SPDB 98+%
10mg
$ 112.00

ChemScene
SPDB 99.30%
5mg
$ 108.00

ChemScene
SPDB 99.30%
10mg
$ 144.00

Total 20 raw suppliers

Chemical Property of N-Succinimidyl 4-(2-pyridyldithio)butanoate

Chemical Property:

PSA：0.00000
LogP:0.00000
Storage Temp.:Sealed in dry,Store in freezer, under -20°C
XLogP3:1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:8
Exact Mass:326.03949928
Heavy Atom Count:21
Complexity:390

Purity/Quality:

99%, ^*data from raw suppliers

4-(Pyridin-2-yldisulfanyl)butyric acid N-Hydroxysuccinimide ester 90+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CC(=O)N(C1=O)OC(=O)CCCSSC2=CC=CC=N2

Technology Process of N-Succinimidyl 4-(2-pyridyldithio)butanoate

There total 4 articles about N-Succinimidyl 4-(2-pyridyldithio)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.65%

: 250266-79-6
4-(pyridin-2-yldisulfanyl)butanoic acid

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 115088-06-7
2,5-dioxopyrrolidin-1-yl 4-(pyridin-2-yldisulfanyl)butanoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl acetamide; at 25 ℃; for 1h;

Reference yield: 84.8%

: 74124-79-1
di(succinimido) carbonate

: 1229158-84-2
C₉H₁₁NO₂S₂*C₁₂H₂₃N

: 115088-06-7
2,5-dioxopyrrolidin-1-yl 4-(pyridin-2-yldisulfanyl)butanoate

Guidance literature:: In methyl isobutyl ketone (MIBK); at 0 - 20 ℃; for 4.5h;

Reference yield:

: 2127-03-9
2,2'-dipyridyldisulphide

: 115088-06-7
2,5-dioxopyrrolidin-1-yl 4-(pyridin-2-yldisulfanyl)butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / acetic acid / ethanol; ethyl acetate / 2 h

2: 31 percent / 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide*HCl / CH₂Cl₂ / 2 h

With acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm060319f