Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate

Base Information

Chemical Name:Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate
CAS No.:802541-47-5
Molecular Formula:C₁₃H₁₈O₅
Molecular Weight:254.283
Hs Code.:
Mol file:802541-47-5.mol

Synonyms:ETHYL 2-(3-METHOXY-6,6-DIMETHYL-2-OXOCYCLOHEX-3-EN-1-YL)-2-OXOACETATE;3-Cyclohexene-1-acetic acid, 3-methoxy-6,6-dimethyl-α,2-dioxo-, ethyl ester

Suppliers and Price of Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Crysdot
Ethyl2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate 95+%
1g
$ 474.00

Total 1 raw suppliers

Chemical Property of Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate

Chemical Property:

Boiling Point:379.9±42.0 °C(Predicted)
PKA:6.39±0.60(Predicted)
Density:1.14±0.1 g/cm3(Predicted)

Purity/Quality:: Ethyl2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate 95+% ^*data from reagent suppliers

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Technology Process of Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate

There total 2 articles about Ethyl 2-(3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)-2-oxoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-92-1
oxalic acid diethyl ester

: 802541-47-5
ethyl (3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)(oxo)acetate

Guidance literature:: 2-methoxy-5,5-dimethylcyclohex-2-en-1-one; With sodium hydride; In tetrahydrofuran; for 0.25h;

oxalic acid diethyl ester; In tetrahydrofuran; for 1h; Heating / reflux;

Reference yield:

: 85312-29-4
2-methoxy-5,5-dimethylcyclohex-2-en-1-one

: 95-92-1
oxalic acid diethyl ester

: 802541-47-5
ethyl (3-methoxy-6,6-dimethyl-2-oxocyclohex-3-en-1-yl)(oxo)acetate

Guidance literature:: 2-methoxy-5,5-dimethylcyclohex-2-en-1-one; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.25h; Inert atmosphere;

oxalic acid diethyl ester; In tetrahydrofuran; mineral oil; for 1h; Reflux;
DOI:10.1021/jm9006559