3-Chloroazocan-2-one

Base Information

Chemical Name:3-Chloroazocan-2-one
CAS No.:32566-60-2
Molecular Formula:C₇H₁₂ClNO
Molecular Weight:161.631
Hs Code.:2933790090
Mol file:32566-60-2.mol

Synonyms:3-chloroazocan-2-one;3-Chlorohexahydro-2(1H)-azocinone;2(1H)-Azocinone, 3-chlorohexahydro-

Suppliers and Price of 3-Chloroazocan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3-Chloroazocan-2-one 97%
1g
$ 451.00

Total 9 raw suppliers

Chemical Property of 3-Chloroazocan-2-one

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:328.071°C at 760 mmHg
Flash Point:152.212°C
PSA：32.59000
Density:1.131g/cm³
LogP:1.55990

Purity/Quality:

97% ^*data from raw suppliers

3-Chloroazocan-2-one 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Chloroazocan-2-one

There total 4 articles about 3-Chloroazocan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 26228-96-6
3,3-dichlorohexahydroazocin-2(1H)-one

: 32566-60-2
3-chlorohexahydroazocin-2(1H)-one

Guidance literature:: With hydrogen; sodium acetate; palladium 10% on activated carbon; In acetic acid; at 20 ℃; for 18h;

Reference yield:

: 502-42-1
cycloheptanone

: 32566-60-2
3-chlorohexahydroazocin-2(1H)-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydroxylamine hydrochloride; pyridine / 0 - 20 °C

2.1: phosphorus pentoxide / water / 1 h / 130 - 140 °C

3.1: phosphorus pentachloride / dichloromethane; toluene / 2 h / Reflux

3.2: 16 h / pH 8 / Cooling with ice

4.1: hydrogen; sodium acetate / palladium 10% on activated carbon / acetic acid / 18 h / 20 °C

With pyridine; phosphorus pentoxide; phosphorus pentachloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; palladium 10% on activated carbon; In dichloromethane; water; acetic acid; toluene;

Reference yield:

: 673-66-5
7-amino-heptanoic acid lactam

: 32566-60-2
3-chlorohexahydroazocin-2(1H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: phosphorus pentachloride / dichloromethane; toluene / 2 h / Reflux

1.2: 16 h / pH 8 / Cooling with ice

2.1: hydrogen; sodium acetate / palladium 10% on activated carbon / acetic acid / 18 h / 20 °C

With phosphorus pentachloride; hydrogen; sodium acetate; palladium 10% on activated carbon; In dichloromethane; acetic acid; toluene;