2,6-DIMETHYL-4-FLUOROBENZALDEHYDE

Base Information

• Chemical Name: 2,6-DIMETHYL-4-FLUOROBENZALDEHYDE
• CAS No.: 925441-35-6
• Molecular Formula: C9H9FO
• Molecular Weight: 152.168
• Hs Code.: 2913000090
• Mol file: 925441-35-6.mol

Synonyms:5-Fluoro-3-formyl-m-xylene;

Chemical Property of 2,6-DIMETHYL-4-FLUOROBENZALDEHYDE

Chemical Property:

• Boiling Point: 229.5±35.0 °C(Predicted)
• PSA: 17.07000
• Density: 1.103±0.06 g/cm3(Predicted)
• LogP: 2.25500
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

4-Fluoro-2,6-dimethylbenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,6-DIMETHYL-4-FLUOROBENZALDEHYDE

There total 2 articles about 2,6-DIMETHYL-4-FLUOROBENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2‐bromo‐5‐fluoro‐1,3‐dimethylbenzene (14659-58-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-fluoro-2,6-dimethylbenzaldehyde (925441-35-6)

Guidance literature:

2‐bromo‐5‐fluoro‐1,3‐dimethylbenzene; With n-butyllithium;

N,N-dimethyl-formamide;

DOI:10.1021/jacs.7b13037

Reference yield:

→ 4-fluoro-2,6-dimethylbenzaldehyde (925441-35-6)

Guidance literature:

With sodium tetrahydridoborate; In methanol; for 0.5h; Inert atmosphere; Cooling with ice;

Reference yield: 89.0%

4-fluoro-2,6-dimethylbenzaldehyde (925441-35-6) + aniline (62-53-3) → 1-(4-fluoro-2,6-dimethylphenyl)-N-phenylmethanimine

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 18h; Molecular sieve; Reflux;

DOI:10.1055/s-0040-1720349

upstream raw materials:

2‐bromo‐5‐fluoro‐1,3‐dimethylbenzene

N,N-dimethyl-formamide

Downstream raw materials:

2,6-dimethyl-4-phenoxy-benzaldehyde

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