Technology Process of 4-AMino-7-broMo-thieno[3,...
There total 5 articles about 4-AMino-7-broMo-thieno[3,... which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
ammonia;
In
isopropyl alcohol;
at 95 - 100 ℃;
for 7h;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: bromine / acetic acid / 10 h / 120 °C / sealed reactor
2: trichlorophosphate / 3 h / 150 °C
3: ammonia / isopropyl alcohol / 12 h / 100 °C / sealed vessel
With
ammonia; bromine; trichlorophosphate;
In
acetic acid; isopropyl alcohol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: trichlorophosphate / 3 h / 150 °C
2: ammonia / isopropyl alcohol / 12 h / 100 °C / sealed vessel
With
ammonia; trichlorophosphate;
In
isopropyl alcohol;