2-(Allyloxy)ethyl acetoacetate

Base Information

Chemical Name:2-(Allyloxy)ethyl acetoacetate
CAS No.:77757-00-7
Molecular Formula:C9H14O4
Molecular Weight:186.21
Hs Code.:
Mol file:77757-00-7.mol

Synonyms:3-oxo-hex-5-enyl acetoacetate;2-(Allyloxy)ethyl acetoacetate;2-(Allyloxy)ethyl acetoacetate,3-oxo-hex-5-enyl acetoacetate

Suppliers and Price of 2-(Allyloxy)ethyl acetoacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(Allyloxy)ethyl acetoacetate

Chemical Property:

PSA：52.60000
LogP:0.71130

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(Allyloxy)ethyl acetoacetate

There total 1 articles about 2-(Allyloxy)ethyl acetoacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 111-45-5,27274-31-3
ethylene glycol monoallyl ether

: 5394-63-8
2,2,6-trimethyl-4H-1,3-dioxin-4-one

: 77757-00-7
3-Oxo-butyric acid 2-allyloxy-ethyl ester

Guidance literature:: In xylene; for 1.5h; Heating;
DOI:10.1016/S0040-4020(98)83021-4

Reference yield:

: 77757-00-7
3-Oxo-butyric acid 2-allyloxy-ethyl ester

: 204522-68-9
C₁₃H₁₄Cl₂N₂O₃

Guidance literature:: Multi-step reaction with 2 steps

1: 41 percent / SO₂Cl₂ / CHCl₃ / 2 h / Ambient temperature

2: 46 percent / NaOAc / methanol; H₂O / Ambient temperature; pH 5, overnight

With sulfuryl dichloride; sodium acetate; In methanol; chloroform; water;
DOI:10.1016/S0040-4020(98)83021-4