3'-O-tert-Butyldimethylsilyladenosine

Base Information

• Chemical Name: 3'-O-tert-Butyldimethylsilyladenosine
• CAS No.: 69504-14-9
• Molecular Formula: C16H27N5O4Si
• Molecular Weight: 381.5
• Mol file: 69504-14-9.mol

Synonyms:3'-O-(tert-butyldimethylsilyl)adenosine;O3'-(tert-butyl-dimethyl-silanyl)-adenosine;

Chemical Property of 3'-O-tert-Butyldimethylsilyladenosine

Chemical Property:

• PSA: 128.54000
• LogP: 1.63070

Purity/Quality:

97% ^*data from raw suppliers

3'-O-tert-Butyldimethylsilyladenosine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3'-O-tert-Butyldimethylsilyladenosine

There total 4 articles about 3'-O-tert-Butyldimethylsilyladenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

3',5'-bis-O-(tert-butyldimethylsilyl)-β-D-adenosine (69504-03-6) → 3'-O-(tert-butyldimethylsilyl)adenosine (69504-14-9)

Guidance literature:

With ammonium cerium(IV) nitrate; silica gel; In tetrachloromethane; isopropyl alcohol; for 9h; Heating;

DOI:10.1021/jo000024o

Reference yield: 76.0%

3'-O-tert-butyldimethylsilyl-5'-O-triethylsilyl-2'-deoxy-adenosine (1237843-27-4) → 3'-O-(tert-butyldimethylsilyl)adenosine (69504-14-9)

Guidance literature:

With methanol; formic acid; at 5 - 20 ℃; chemoselective reaction; Inert atmosphere;

DOI:10.1080/15257770903362172

Reference yield:

2'-O-(tert-butyldimethylsilyl)adenosine (69504-13-8) → 3'-O-(tert-butyldimethylsilyl)adenosine (69504-14-9)

Guidance literature:

In methanol; at 30 ℃; Rate constant; half time of isomerisation;

DOI:10.1016/S0008-6215(00)85245-3

upstream raw materials:

2'-O-(tert-butyldimethylsilyl)adenosine

3',5'-bis-O-(tert-butyldimethylsilyl)-β-D-adenosine

3'-O-tert-butyldimethylsilyl-5'-O-triethylsilyl-2'-deoxy-adenosine

Downstream raw materials:

2'-O-(tert-butyldimethylsilyl)adenosine

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