2-METHYLPROPENE-1-13C

Base Information

• Chemical Name: 2-METHYLPROPENE-1-13C
• CAS No.: 71910-43-5
• Molecular Formula: (CD3)3CD
• Molecular Weight: 68.18
• Mol file: 71910-43-5.mol

Synonyms:Benzaldehyde-carbonyl-13C,D;(carbonyl-13C,2H)benzaldehyde;[1-(13)C,(2)H]-benzaldehyde;2-methyl-[1-13C]propene;1-(13)C-isobutene;Benzaldehyde-|A-13C,|A-d1;1-13C-isobutylene;2-methylpropene-1-(13)C;1-13C-2-methylpropene;isobutylene-1-13C;

Chemical Property of 2-METHYLPROPENE-1-13C

Chemical Property:

• PSA: 0.00000
• LogP: 1.58240

Purity/Quality:

97% ^*data from raw suppliers

2-Methylpropene-1-13C(gas) ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-METHYLPROPENE-1-13C

There total 2 articles about 2-METHYLPROPENE-1-13C which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[13C]-methyltriphenylphosphonium iodide (81826-67-7) + acetone (67-64-1) → 1-13C-2-methylpropene (71910-43-5)

Guidance literature:

[13C]-methyltriphenylphosphonium iodide; With dimsylsodium; In dimethyl sulfoxide; for 1h;

acetone; In dimethyl sulfoxide; at 60 ℃; for 0.25h;

DOI:10.1021/ja0496975

Reference yield:

→ 1-13C-2-methylpropene (71910-43-5)

Guidance literature:

¹³C-Methyltriphenylphosphoniumiodid, n-BuLi, Aceton;

DOI:10.1021/ja00482a027

upstream raw materials:

[13C]-methyltriphenylphosphonium iodide

acetone